Isolation, Purification, and Characterization of Cyclomaltodecaose (ε-Cyclodextrin), Cyclomaltoundecaose (ζ-Cyclodextrin) and Cyclomaltotridecaose (θ-Cyclodextrin)
スポンサーリンク
概要
- 論文の詳細を見る
Cyclomaltodecaose (ε-cyclodextrin, ε-CD), cyclomaltoundecaose (ζ-CD) and cyclomaltotridecaose (θ-CD) are a series of cyclomalto-oligosaccharides composed of ten, eleven and thirteen α-(1→4)-linked D-glucopyranose units, respectively. ε-CD, ζ-CD and θ-CD were purified from the commercially available CD powder mainly using the combined treatment of HPLC and column chromatographies. The molecular weights of ε-CD, ζ-CD and θ-CD were determined by FAB-MS, and their cyclic structures were identified by ^1H-NMR and ^<13>C-NMR. Furthermore, the ^<13>C-NMR chemical shift of large-ring cyclodextrins composed of several α-(1→4)-linked D-glucopyranose units, in which numbers 9,10,11,12,and 13 are named δ-, ε-, ζ-, η-, θ-CD, were elucidated and compared with those of conventional α-, β-, and γ-CD.
- 社団法人日本薬学会の論文
- 1997-03-15
著者
-
Nagase Hidetaka
大鵬薬品工業
-
Endo T
Graduate School Of Pharmaceutical Sciences Hokkaido University
-
Endo T
Department Of Physical Chemistry Hoshi University
-
Endo Tomohiro
Department of Materials, Physics and Energy Engineering, Nagoya University
-
Nagai T
Department Of Pharmaceutics Hoshi University
-
NAGASE Hiromasa
Department of Physical Chemistry, Hoshi University
-
UEDA Haruhisa
Department of Physical Chemistry, Hoshi University
-
NAGAI Tsuneji
Faculty of Pharmaceutical Sciences, Hoshi University
-
KOBAYASHI Shoichi
Akita Research Institute of Food & Brewing
-
Ueda H
Kyoto Pharmaceutical University
-
Kobayashi S
Eisai Research Institute Of Boston Inc.
-
Ueda H
Hoshi Univ. Tokyo Jpn
-
Ueda H
Department Of Physical Chemistry Hoshi University
-
Ueda H
Faculty Of Pharmaceutical Sciences Hoshi University
-
Ueda Haruhisa
Faculty Of Pharmaceutical Science Hoshi University
-
Ueda Haruhisa
Department Of Physical Chemistry Hoshi University
-
Kobayashi Shoichi
Laboratory Of Food And Health Science Department Of Agro-bioscience Faculty Of Agriculture Iwate Uni
-
Ueda Hideo
Fac. Of Pharmaceutical Sciences Josai Univ.
-
Kobayashi Shigeki
Department Of Analytical Chemistry Of Medicines Showa Phamaceutical University
-
Ueda H
Fac. Of Pharmaceutical Sciences Josai Univ.
-
Kobayashi Shigeki
Department Of Analytical Chemistry Of Medicines Showa Pharmaceutical University
-
Kobayashi Shigeki
Div. Of Analytical Chemistry Of Medicines Showa Pharmaceutical Univ.
-
Nagase H
Pharmacobioregulation Research Laboratory Taiho Pharmaceutical Co. Ltd.
-
Nagai Tsuneji
Faculty Of Pharmaceutical Sciences Hoshi University
-
Endo Tomohiro
Department Of Material Physics And Energy Engineering Graduate School Of Engineering Nagoya Universi
-
Endo Tomohiro
Department Of Functional Radiation Sciences Hoshi University
関連論文
- PJ-573 Dantrolene Prevents Catecholaminergic Polymorphic Ventricular Tachycardia (CPVT) by Correcting Abnormal Ca^ Release through the Ryanodine Receptor(PJ096,Arrhythmia, Others (Clinical/Pathophysiology) 4 (A),Poster Session (Japanese),The 73rd Annu
- Cell Type-Dependent Divergence of Transactivation by Glucocorticlid Receptor Ligand
- In Vivo Analysis of Glucocorticoid-Induced Reporter Gene Expression Using Gene Gun DNA Delivery
- 3 Correction of RyR2 Defects as a New Therapeutic Strategy against Heart Failure(Novel Therapeutic Strategies against Heart Failure,KSC-JCS Joint Symposium (KSC-JCS Joint Symposium) (I),The 73rd Annual Scientific Meeting of The Japanese Circulation Societ
- α-アドレナリン遮断作用を有するアポガランタミン類似体のConformationについて
- 環境ホルモンの電子構造はその毒性や生物活性の発現にどのような相関性を持つのであろうか?-ハードネス概念の生物学への応用-
- Alkaloidal Constituents of Leucojum autumnale L. (Amaryllidaceae)
- Isolation and Structure Elucidation of a Novel Alkaloid, Incartine, a Supposed Biosynthetic Intermediate, from Flowers of Lycoris incarnata
- Alkaloidal Constituents of Hymenocallis rotata HERB. (Amaryllidaceae)(Organic,Chemical)
- Structures of Acid B and Related Compounds, Oxidation Products of Lycoramine
- Alkaloidal Constituents of Leucojum asetivum L. (Amaryllidaceae)
- Alkaloidal Constituents of Crinum latifolium and Crinum bulbispermum (Amaryllidaceae)
- Isolation of O-Demethyllycoramine from Bulbs of Lycoris radiata HERB.
- Transformation of Tazettine to Pretazettine
- Improvement of Tone’s Method with Two-Term Rational Approximation
- Explicit Time Integration Scheme Using Krylov Subspace Method for Reactor Kinetics Equation
- Relationship between the Biological Potency of Polychlorinated Dibenzo-p-dioxins and Their Electronic States
- Isolation, Purification and Characterization of Cyclomaltooctadecaose (v-Cyclodextrin), Cyclomaltononadecaose (ζ-Cyclodextrin), Cyclomaltoeicosaose (o-Cyclodextrin) and Cyclomaltoheneicosaose (π-Cyclodextrin)
- Isolation, Purification, and Characterization of Cyclomaltotetradecaose (ι-Cyclodextrin), Cyclomaltopentadecaose (κ-Cyclodextrin), Cyclomaltohexadecaose (λ-Cyclodextrin), and Cyclomaltoheptadecaose(μ-Cyclodextrin)
- Complex Formation of Cyclomaltononaose δ-Cyclodextrin (δ-CD) with Macrocyclic Compounds
- Polymorphic Structure of dl-12Hydroxystearic Acid
- Crystal Structure of Cyclomaltodecaose(ε-Cyclodextrin)at 203 K
- Solubilization of C_ into Water by Complexation with δ-Cyclodextrin
- Isolation and Purification of Cyclomaltononaose (δ-CD) from CELDEX SG-30
- Isolation, Purification, and Characterization of Cyclomaltodecaose (ε-Cyclodextrin), Cyclomaltoundecaose (ζ-Cyclodextrin) and Cyclomaltotridecaose (θ-Cyclodextrin)
- Crystal Structure of DL-12-Hydroxystearic Acid
- Medicinal Foodstuffs.XXVII.^ Saponin Constituents of Gotu Kola(2) : Structures of New Ursane- and Oleanane-Type Triterpene Oligoglycosides, Centellasaponins B, C, and D, from Centella asiatica Cultivated in Sri Lanka
- Medicinal Foodstuffs(26)Inhibitors of Aldose Reductase and New Triterpene and Its Oligoglycoside, Centellasapogenol A and Centellasaponin A, from Centella asiatica(Gotu Kola)
- Piperidine Carboxylic Acid Derivatives of 10H-Pyrazino[2,3-b][1,4] benzothiazine as Orally-Active Adhesion Molecule Inhibitors
- Inhibitors of Adhesion Molecules Expression : The Synthesis and Pharmacological Properties of 10H-Pyrazino [2,3-b] [1,4] benzothiazine Derivatives
- SYNTHESIS AND BIOLOGICAL ACTIVITIES OF BIOISOSTERIC O-CARBA-ANALOGUES OF PLATELET ACTIVATING FACTOR (PAF)
- Spectroscopic Study on Interaction of Nucleic Acid Base with Tryptophan-Containing Tripeptides : Acetyl-Trp-X-Trp-NHCH_3 (X=Gly, Asn, Asp, Gln and Glu)
- Sequence-Dependent Interaction of Acidic Amino Acid with Guanine Base in Tryptophan-Containing Dipeptides : Spectroscopic Studies
- Study on Preparation and Formation Mechanism of n-Alkanol/Water Emulsion Using α-Cyclodextrin
- A Modified Method Using Static Head-Space Gas Chromatography for Determining the Stability Constants of 1-Alkanol/α-Cyclodextrin Complexation
- Enhancement of Water Solubility of Fullerene by Cogrinding with Mixture of Cycloamyloses, Novel Cyclic α-1,4-Glucans, via Solid-Solid Mechanochemical Reaction
- Development of New Solid Angle Quadrature Sets to Satisfy Even- and Odd-Moment Conditions
- Isolation of N-Demethylgalanthamine from the Bulbs of Crinum asiaticum L. var. japanicum BAKER (Amaryllidaceae)
- Dissolution Properties of Indomethacin from Coprecipitates with Water-Insoluble Glucan(Pharmaceutical)
- Production and Physicochemical Properties of Water-Insoluble Glucan from Streptococcus mutans(Pharmaceutical)
- Ability of Poly-L-arginine to Enhance Drug Absorption into Aqueous Humor and Vitreous Body after Instillation in Rabbits(Biopharmacy)
- Influence of Skin Hydration on Anesthetic Effect of Lidocaine Tape in Hemodialysis Patients
- Effects of Poly-L-arginine on the Permeation of Hydrophilic Compounds through Surface Ocular Tissues(Biopharmacy)
- Investigation of the Release Test Method for the Topical Application of Pharmaceutical Preparations : Release Test of Cataplasm Including Nonsteroidal Anti-inflammatory Drugs Using Artificial Sweat
- Synthetic Studies of Zoanthamine/Norzoanthamine : Biogenetic-like One-Step Construction of the Heterocyclic Aminal Core (CDEFG Ring) from a Monocyclic Precursor
- Glycosyl 2-Pyridinecarboxylate as an Effective Glycosyl Donor : Glycosidation of Mannose, 2-Azidosugar, and 2-Deoxysugar into Disaccharides
- Amphidinin B, a New Polyketide Metabolite from Marine Dinoflagellate Amphidinium sp.
- Application of Modified Mosher's Method for Primary Alcohols with a Methyl Group at C2 Position
- Liver Targeting Liposomes Containing β-Sitosterol Glucoside with Regard to Penetration-Enhancing Effect on HepG2 Cells
- Physicochemical Characteristics and Transfection Efficiency of DNA in Liposomes with Soybean-Derived Sterylglucoside into HepG2 Cells
- Electron Spin Resonance Studies of Dipalmitoylphosphatidylcholine Liposomes Containing Soybean-Derived Sterylglucoside
- High Entrapment of Insulin and Bovine Serum Albumin into Neutral and Positively-Charged Liposomes by the Remote Loading Method
- High Absorbency and Subchronic Morphologic Effects on the Nasal Epithelium of a Nasal Insulin Powder Dosage Form with a Soybean-derived Sterylglucoside Mixture in Rabbits
- Nasal Insulin Delivery in Rabbits Using Soybean-Derived Sterylglucoside and Sterol Mixtures as Novel Enhancers in Suspension Dosage Forms
- Targeting of Soybean-Derived Sterylglucoside Liposomes to Liver Tumors in Rat and Mouse Models
- Formulation of Liposomes with a Soybean-Derived Sterylglucoside Mixture and Cholesterol for Liver Targeting
- Separation of Stereoisomers of Some Terpene Derivatives by Capillary Gas Chromatography-Mass Spectrometry and High-Performance Liquid Chromatography Using β-Cyclodextrin Derivative Columns
- Analyses of Anandamide and Endocannabinoid-like Compounds Using Collision-induced Dissociation in Fast Atom Bombardment Ionization-Mass Spectrometry and Gas Chromatography/Chemical Ionization-Mass Spectrometry
- Poly(ethylene glycol) Derivative of Cholestrol Reduces Binding Step of Liposome Uptake by Murine Macrophage-like Cell Line J774 and Human Hepatoma Cell Line HepG2
- Association of Liposomes Containing a Soybean-Derived Sterlyglucoside Mixture with Rat Primary Cultured Hepatocytes
- Rational Drug Design and Synthesis of a Highly Selective Nonpeptide δ-Opioid Agonist, (4aS^*, 12aR^*)-4a-(3-Hydroxyphenyl)-2-methyl-1,2,3,4,4a, 5,12,12a-octahydropyrido[3,4-b]acridine (TAN-67)
- DISCOVERY OF A STRUCTURALLY NOVEL OPIOID K-AGONIST DERIVED FROM 4,5-EPOXYMORPHINAN
- NOR-BINALTORPHIMINE (NOR-BNI) : POTENT AND SELECTIVE KAPPAOPIOID RECEPTOR ANTAGONIST WITH LONG-LASTING ACTIVITY IN VIVO
- Synthesis of 2'-Cyanomethyl-2-biphenylcarboxylic Acid
- In Vivo Drug Release and Antitumor Characteristics of Water-Soluble Conjugates of Mitomycin C with Glycol-Chitosan and N-Succinyl-Chitosan
- Preparation and Drug Release Characteristics of the Conjugates of Mitomycin C with Glycol-chitosan and N-Succinyl-chitosan
- Preparation and Evaluation of the Macromolecular Conjugate of 2' or3'-(4-Carboxybutyryl)doxifluridine with Chitosan
- Simultaneous Determination of the Stability Constants for Fragrance Materials with 2-Hydroxypropyl-β-Cyclodextrin by Static Head-Space Gas Chromatography
- Solubility Method Using Static Head-Space Gas Chromatography for Determination of the Stability Constants of Fragrance Materials with 2-Hydroxypropyl-β-cyclodextrin
- A New Competitive Method Using Static Head-Spece Gas Chromatography for the Determination of Cyclodextrin Complex Stability Constants
- Determination of the Stability Constants of Benzene and Alkylbenzenes with α-Cyclodextrin by Static Head-Space Gas Chromatography
- Acoustic Cavitation as an Enhancing Mechanism of Low-Frequency Sonophoresis for Transdermal Drug Delivery
- Effects of Sonication on the Lamellar Structures of L-α-Dipalmitoyl Phosphatidylcholine(DPPC)/Saccharide/Water Systems
- Relationship between Hydrophobic Index of Saccharide and Gel-Liquid Crystal Transition Temperature of the L-α-Dipalmitoyl Phosphatidylcholine (DPPC)/Saccharide/Water System
- Synthesis, Conformation, and Chemical Properties of New Mini Parallel Double-Stranded Peptides Conjugated with -Phe-Phe- and -Phe-Phe-X- Sequences
- Diastereomer-Specific Effects of Double-Stranded Peptides Conjugated with-L-Tyr-L-Phe-or-L-Tyr-D-Phe-Residues on Tyrosine : Phosphorylation and Inhibition of src^NRK, A431, MCF-7, and DU145 Cell Growth
- Diastereomeric Selective Effects of Double-Stranded Peptides Conjugated with -Phe-Phe- Residue for Growth Inhibition and Permeability of Ca^ on A431, src^NRK, and A549 Cells Proliferation
- Development of Soft-Based Double-Stranded Peptide Chelators which Selectively Separate Europium and Lanthanum Ions Based on the Hardness Concept(Communications to the Editor)
- Development of Functional Double-stranded Peptide Chelators Which Selectively Separate Europium and Lanthanum Ions
- Bioavailability of Theophylline and Thiamine Disulfide Incorporated into Mucoadhesive Microspheres Consisting of Dextran Derivatives and Cellulose Acetate Butyrate (Biopharmacy)
- Effect of Mixed Micelle Formulations Including Terpenes on the Transdermal Delivery of Diclofenac (Biopharmacy)
- Promoting Mechanism of Menthol Derivative, 1-O-Ethyl-3-buthylcyclohexanol, on the Percutaneous Absorption of Ketoprofen
- In Vitro Drug Release from Macromolecule-Drug Conjugates of 3'-(7-Carboxyheptanoyl)-5-fluoro-2'-deoxyuridine with Decylenediamine-dextran T70 of Poly-L-lysine(Pharmaceutical)
- Enhancing Effect of Switching Iontophoresis on Transdermal Absorption of Sodium Benzoate In Vivo
- DNA Topology on an Increase in Positive Writhing Number of DNA : Conformation Changes in the Time Course of cis-Diamminedichloroplatinum(II)-DNA Adducts
- Enhancement of in Vivo Anti-influenza Virus Activity of 5,7,4'-Trihydroxy-8-methoxyflavone by Drug Delivery System Using Hydroxypropyl Cellulose
- Drug Permeation Behavior in Chitosan Film Prepared on the Metal Plate Loaded with Electric Charge
- Application of the Robust Design Concept for Fuel Loading Pattern
- Improvement of Tone's Method with Two-Term Rational Approximation
- Explicit Time Integration Scheme Using Krylov Subspace Method for Reactor Kinetics Equation
- Diastereomeric Selective Effects for Growth Inhibition of Synthesized Mini Parallel Double-Stranded Peptides on Escherichia coli and Staphylococcus aureus
- Topology Effect for DNA Structure of Cisplatin : Topological Transformation of Cisplatin-Closed Circular DNA Addusts by DNA Topoisomerase I
- Hardness Controlled Enzymes and Electronegativity Controlled Enzymes : Role of an Absolute Hardness-Electronegativity (η-χ) Activity Diagram as a Coordinate for Biological Activities
- Stereo Structure-Controlled and Electronic Structure-Controlled Estrogen-Like Chemicals to Design and Develop Non-estrogenic Bisphenol A Analogs Based on Chemical Hardness Concept
- Isolation of Clivacetine from Clivia miniata REGEL. (Amaryllidaceae)
- Isolation of Carinatine and Pretazettine from the Bulbs of Zephyranthes carinate HERB. (Amaryllidaceae)
- 10-Hydroxy-9-phenanthrenecarbonitrile誘導体の新合成法
- Synthesis of optically Active Deoxytazettine Neomethine
- Suitability of Synthetic Copolymer Membranes as a Human Skin Alternative for In Vitro Skin Permeation Testing
- Trends in the Development of Biofunctional Saccharides in Japan.