Peptides Containing Aminophosphonic Acids. II. The Synthesis of Tripeptide Analogs
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概要
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The synthesis of tripeptides containing aminophosphonic acid was attempted as follows. Diethyl phthalylimidomethyl phosphonate (I) was chlorinated with phosphorus pentachloride to the phosphonomonochloridate (II), which was then coupled with amino acid ethyl esters to give the corresponding dipeptides (IIIa—c). The phthalyl groups of III were removed with hydrazine, and the resulting free amines were subsequently combined with phthalyl-amino acids by means of dicyclohexylcarbodiimide to produce the tripeptide analogs (IVa—c) in good yields.
- 公益社団法人 日本化学会の論文
著者
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Yamauchi Kiyoshi
Department Of Bioapplied Chemistry Faculty Of Engineering Osaka City University
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Imoto Minoru
Department of Applied Chemistry Faculty of Engineering Osaka City University
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Kinoshita Masayoshi
Department of Applied Chemistry, Faculty of Engineering, Osaka City University
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