Archaebacterial Lipids:Surface Pressure-Surface Area Isotherms of 1,1'-(1,32-Dotriacontanediyl)bis(2-((3RS,7R,11R)-3,7,11,15-tetramethylhexadecyl)-sn-glycero-3-phosphocholine).
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概要
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1,1′-(1,32-Dotriacontanediyl)bis[2-[(3<I>RS</I>,1<I>R</I>,11<I>R</I>)-3,7,11,15-tetramethylhexadecyl]-<I>sn</I>-glycero-3-phosphocholine] (the tetramethylhexadecyl group=phytanyl) was synthesized conveniently by reactions involving etherification of 1,1′-(1,32-dotriacontanediyl)bis(3-benzyl-<I>sn</I>-glycerol) (<B>1</B>) with (7<I>R</I>,11<I>R</I>)-3,7,11,15-tetramethyl-2-hexadecenyl bromide and hydrogenation of the resulting unsaturated ether with <I>p</I>-tolylsulfonylhydrazine; a total yield from <B>1</B>, 7–10%. Unlike usual monopolar double-chain-amphiphiles, the bipolar lipid bent into a U-form in a water–air interface to produce the Langmuir membrane, exhibiting peculiar surface pressure–surface area isotherms.
- 公益社団法人 日本化学会の論文
著者
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Kamikawa Tadao
Department Of Chemistry Faculty Of Science And Technology Kinki University
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Yamauchi Kiyoshi
Department Of Bioapplied Chemistry Faculty Of Engineering Osaka City University
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Kinoshita Masayoshi
Department of Applied Chemistry, Faculty of Engineering, Osaka City University
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Yamada Katsu
Department of Bioapplied Chemistry, Faculty of Engineering, Osaka City University
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