The crystal and molecular structure of 2,3,6,8,9-pentaphenyl-1-thia-6-azaspiro(4.4)nona-2,8-diene-4,7-dione.

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概要

• 論文の詳細を見る

• The title compound crystallizes in monoclinic form, space group P2<SUB>1</SUB>/c with <I>a</I>=20.810(1), <I>b</I>=16.000(1), <I>c</I>=18.131(1) Å, β=107.77(1)°, <I>Z</I>=8. The structure was established by the direct method and refined including all hydrogen atoms by the blockdiagonal least-squares procedure, <I>R</I>=0.062 for 4609 observed reflections. The heterocyclic spiran skeletons in two independent molecules have the same structure; however, four phenyl rings out of five take different conformations to the hetero rings to which they attached.

• 公益社団法人 日本化学会の論文

著者

• Kai Yasushi

  Department Of Applied Chemistry Faculty Of Engineering Osaka University

• Kasai Nobutami

  Department Of Applied Biological Science Tokyo University Of Science

• Yasuoka Noritake

  Department Of Life Science Faculty Of Science Himeji Institute Of Technology

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