A New Fluorometric Analysis of Dulcin using Sodium Nitrite. III. Structural Determination of the Fluorescent Compound by the Single Crystal X-Ray Diffraction Method

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概要

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• The structure of the fluorescent compound (A) obtained from the reaction of dulcin and sodium nitrite was previously presumed to be 1,3-bis (4-ethoxyphenyl)-5-tetrazolone. In this paper, (2-bromoethoxy) phenyl derivative (B) which has the same structural skeleton of compound A was synthesized and analized by the single crystal X-ray diffraction method to determine the structure more conclusively. The structure of compound B was discussed on the basis of the result of the two-dimensional analysis. The structure of the fluorescent compound A was consequently concluded as 1,3-bis (4-ethoxyphenyl)-5-tetrazolone.

• 公益社団法人日本薬学会の論文
• 1972-06-25

著者

• 田村 善蔵

  Faculty of Pharmaceutical Sciences, University of Tokyo

• 飯高 洋一

  Faculty of Pharmaceutical Sciences, The University of Tokyo

• 飯高 洋一

  School Of Medicine Teikyo University

• 内山 貞夫

  National Institute of Hygienic Sciences

• 田村 善蔵

  東京大学医学部

• 田村 善蔵

  Faculty Of Pharmaceutical Sciences University Of Tokyo

• 内山 貞夫

  国立衛生試験所

• 飯高 洋一

  Faculty Of Pharmaceutical Sciences The University Of Tokyo

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