The synthesis of highly strained buttaflanes with aromatic rings.

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概要

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• Dibenzo[4.4.2.2]buttaflanes, <I>syn</I>-13,14:15,16-dibenzopentacyclo[6.4.2.2<SUP>2,7</SUP>.0<SUP>1,8</SUP>.0<SUP>2,7</SUP>]hexadeca-13,15-diene, and <I>syn</I>-13,14:15,16-dibenzohexacyclo[6.4.2.2<SUP>2,7</SUP>.0<SUP>1,8</SUP>.0<SUP>2,7</SUP>.0<SUP>3,12</SUP>]hexadeca-13,15-diene were synthesized by the intramolecular photocycloaddition of the dibenzo[<I>a</I>,<I>e</I>]cyclooctene derivatives, <I>syn</I>-13,14:15,16-dibenzotricyclo[6.4.2.2<SUP>2,7</SUP>]hexadeca-1,7,13,15-tetraene and <I>syn</I>-13,14:15,16-dibenzotetracyclo[6.4.2.2<SUP>2,7</SUP>.0<SUP>3,12</SUP>]hexadeca-1,7,13,15-tetraene, which had themselves been derived by the catalytic hydrogenation of the biphenylene photodimer, <I>syn</I>-13,14:15,16-dibenzotricyclo[6.4.2.2<SUP>2,7</SUP>]hexadeca-1,3,5,7,9,11,13,15-octaene, and the pentacyclic compound, <I>syn</I>-13,14:15,16-dibenzopentacyclo[6.4.2.2<SUP>2,7</SUP>.0<SUP>3,12</SUP>.0<SUP>4,11</SUP>]hexadeca-1,5,7,9,13,15-hexaene, respectively.

• 公益社団法人 日本化学会の論文

著者

• Odaira Yoshinobu

  Department Of Applied Fine Chemistry Faculty Of Engineering Osaka University

• Ohno Hideki

  Department Of Gastroenterology Graduate School Of Medicine University Of Tokyo

• Kimura Koji

  Department Of Animal Breeding And Reproduction National Institute Of Livestock And Grassland Science

• Kimura Koji

  Department of Petroleum Chemistry, Faculty of Engineering, Osaka University

• Morikawa Kiyoshi

  Department of Petroleum Chemistry, Faculty of Engineering, Osaka University

• Hiramatsu Yasuhiro

  Department of Petroleum Chemistry, Faculty of Engineering, Osaka University

• OHNO Hideki

  Department of Gastroenterology and Cancer Gene Regulation, Kanazawa University Graduate School of Medical Sciences

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