Mechanical properties of 2.0-3.5mol% Y_2O_3-stabilized zirconia polycrystals fabricated by the solid phase mixing and sintering method
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概要
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The crystal phase and mechanical properties of 2.0 to 3.5mol% Y_2O_3-stabilized zirconia polycrystals sintered from agitator milled powders (solid phase mixing, SPM) were investigated. Powders containing 2.5 and 2.8mol% Y_2O_3 showed higher sinterability than those containing 2.0 and 3.5mol% Y_2O_3. The thermal expansion curve of the 2.5 and 2.8mol% Y_2O_3 samples exhibited a monoclinic to tetragonal phase transformation during the heating stage, with a linear relationship observed during cooling. However, a hysteresis was not observed during the heating and cooling stages when the Y_2O_3 content and sintering temperature were increased. The 2.0mol% Y_2O_3 sample exhibited the transformation and hysteresis, even though the sintering temperature was increased. The relationship between the flexural strength and grain size for the sample with 2.0mol% Y_2O_3 was not linear, but exhibited a peak. The flexural strength of the 2.5 and 2.8mol% Y_2O_3 samples increased as the grain size increased, and then over a certain grain size the flexural strength remained constant and independent of the grain size. The flexural strength and fracture toughness of the 2.0mol% Y_2O_3 sample might be dominated by microcrack-toughening. On the other hand, those for the 2.5 and 2.8mol% Y_2O_3 samples were dependent not only on the stress-induced transformation, but also on the compressive residual stress and microcrack-toughening caused by the transformation. The relationship between the fracture toughness and V_f√<h>, where V_f is the tetragonal phase fraction and h is the transformation depth, for the 2.0, 2.5 and 3.5mol% Y_2O_3 samples was non-linear and exhibited a peak; however, that for the 2.8mol% Y_2O_3 sample was linear.
- 社団法人日本セラミックス協会の論文
- 2008-12-01
著者
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NIIHARA Koichi
Extreme Energy-Density Research Institute, Nagaoka University of Technology
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Sekino Tohru
The Inst. Of Multidisciplinary Res. For Advanced Materials Tohoku Univ.
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Sekino Tohru
Institute Of Multidisciplinary Research For Advanced Materials Tohoku University
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Sekino Tohru
Institute Of Multidisciplinary Research For Advanced Materials (imram) Tohoku University
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Naka Hironori
Nikkato Corporation
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Niihara Koichi
Extreme Energy-density Res. Inst. Nagaoka Univ. Of Technol.
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Ohnishi Hiroshi
Nikkato Corporation
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IKUHARA Yuichi
Institute of Engineering Innovation, University of Tokyo
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Ikuhara Yuichi
Inst. Of Engineering Innovation The Univ. Of Tokyo
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Ikuhara Yuichi
Institute Of Engineering Innovation School Of Engineering The University Of Tokyo
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Ohnishi Hiroshi
Nikkato Corp. Osaka Jpn
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IKUHARA Yuichi
Institute of Engeering Innovation, School of Engineering, The University of Tokyo
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