Studies on Benzodiazepinooxazoles. II. Crystal and Molecular Structure of 10-Bromo-2,3,5,6,7,11b-hexahydro-2-methyl-11b-phenylbenzo [6,7]-1,4-diazepino [5,4-b] oxazol-6-one, C_<18>H_<17>O_2N_2Br・C_2H_5OH
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概要
- 論文の詳細を見る
The crystal structure of 10-bromo-2,3,5,6,7,11b-hexahydro-2-methyl-11b-phenylbenze-[6,7]-1,4-diazepino [5,4-b] oxazol-6-one, C_<18>H_<17>O_2N_2Br・C_2H_5OH, has been determined by the three dimensional Patterson method. This substance occurs as monoclinic crystals, space group P2_1/c, with Z=4 in the unit cell dimensions a=16.34,b=8.88,c=13.89 A, and β=102°. The block-diagonal least-squares refinements using 2780 reflections gave the final R=11.3%. The methyl and phenyl ring substituents are trans with respect to the plane of the oxazole ring.
- 公益社団法人日本薬学会の論文
- 1971-12-25
著者
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宮寺 哲男
Central Research Laboratories, Sankyo Co., Ltd.
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田村 千尋
Central Research Laboratories Sankyo Co., Ltd.
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佐藤 定男
Analytical And Metabolic Research Laboratories Sankyo Co. Ltd.
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佐藤 定男
Central Research Laboratories, Sankyo Co., Ltd.
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宮寺 哲男
Chemical Research Laboratories, Sankyo Co., Ltd.
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桜井 敬子
Central Research Laboratory, Sankyo Co., Ltd.
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大刀川 隆治
Central Research Laboratory, Sankyo Co., Ltd.
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宮寺 哲男
Chemical Research Laboratories Sankyo Co. Ltd.
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大刀川 隆治
Central Research Laboratory Sankyo Co. Ltd.
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桜井 敬子
Central Research Laboratory Sankyo Co. Ltd.
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田村 千尋
Analytical And Metabolic Research Laboratories : Sankyo Company Ltd.
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田村 千尋
Central Research Laboratories Sankyo Co. Ltd.
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