Quantitative Analysis of Sugar Components in Steroidal Saponins by Gas Liquid Chromatography
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概要
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Gas chromatographic determination of monosaccharides such as L-arabinose, L-rhamnose, D-xylose, D-mannose, D-galactose, and D-glucose was studied. The recovery of sugars under hydrolysis condition was examined by GLC (Fig. 1) and was found to be almost quantitative when steroidal glycosides were hydrolyzed with N sulfuric acid in dioxane-water (1 : 3) solution (Table III). A simple and accurate method by GLC was thus presented for the individual determination of sugar components in the micro amounts (5-10 mg) of steroidal saponins. The molar ratios of sugar components were determined on the new convallasaponins by this method (Table V).
- 公益社団法人日本薬学会の論文
- 1968-04-25
著者
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藤間 貞彦
Faculty Of Pharmaceutical Sciences Higashi Nippon Gakuen University
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木村 道也
Faculty Of Pharmaceutical Sciences Hokkaido University
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吉沢 逸雄
Faculty of Pharmaceutical Sciences, Hokkaido University
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服部 保次
Faculty of Pharmaceutical Sciences, Hokkaido University
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