畜肉中の残留有機塩素系農薬及び合成抗菌剤の系統的分析法並びに合成抗菌剤のGC/MSによる確認法の検討

概要

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Organochlorine pesticides as well as synthetic antibacterialagents in cattle meats were extracted with acetonitrile, and the extract was divided into two parts for the individual clean-up. One part of the extract was cleaned up by silica gel column chromatography, and determined by electron capture detecter-gas chromatography (ECD-GC) for organochlorine pesticides. Another part of the extract was cleaned up by washing with n-hexane in the case of edible meats, or by solid phase extraction with Sep-pak Alumina N or tC_<18> mini column in the case of edible viscera, and determined by HPLC with a UV detector for the synthetic antibacterialagents. Recoveries of 7 organochlorine pesticides in edible meats spiked at 0.1 ppm were 54.3-104.6%, and recoveries of 13 antibacterialagents in edible viscera spiked at 0.4 ppm were 59.1-105.3%. Confirmation of nicarbazin (NCZ) in chicken, trimethoprim (TMP) spiked in pork by GC-MS were studied.
公益社団法人日本薬学会の論文
1995-12-31