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概要

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• The light lanthanoid(III) (La or Nd) 1-hydroxy-2-naphthoate crystals indicated in the title were obtained and their structures were determined by the X-ray diffraction method using their single crystals. They are orthorhombic with the space group <I>P</I>2<SUB>1</SUB>2<SUB>1</SUB>2<SUB>1</SUB>, <I>Z</I>=4. The unitcell axis lengths of the lanthanum(III) complex are: <I>a</I>=11.985(4), <I>b</I>=40.21(5), and <I>c</I>=7.017(1) Å. The central metal atom is ennea-coordinated and is in a tricapped trigonal-prism geometry, where two carboxylate ions act as the unidentates, and the other coordinating positions are occupied by water oxygen atoms. The non-coordinated carboxylate ion is hydrogen-bonded to two ligated water oxygen atoms with its respective carboxylato oxygen atoms. The complex molecules are not directly bridged by the carboxylate ions, but the complexes are linked by hydrogenbondings in the a- and c-axis directions. Such hydrophilic and the hydrophobic layers of the naphthalene rings, both of them being parallel to the ac-plane, are laid alternately in the crystal.

• 公益社団法人 日本化学会の論文

著者

• Suzuki Yasuo

  Department Of Applied Physics Faculty Of Engineering Fukui University

• Ouchi Akira

  Department of Chemistry, College of General Education, The University of Tokyo

• Ohki Yoshiyuki

  Department of Industrial Chemistry, Faculty of Engineering, Meiji University

• Ouchi Akira

  Department of Chemistry, College of Arts and Sciences, The University of Tokyo

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