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概要
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The title new complexes were synthesized and their crystal and molecular structures were determined by the single-crystal X-ray diffraction method. The crystal form of [(C<SUB>2</SUB>H<SUB>5</SUB>)<SUB>4</SUB>N]<SUB>3</SUB>[Yb(NCS)<SUB>6</SUB>]·(C<SUB>6</SUB>H<SUB>6</SUB>), for example, is monoclinic, space group <I>P</I>2<SUB>1</SUB>⁄<I>c</I>, <I>a</I>=19.458(12), <I>b</I>=14.046(6), <I>c</I>=18.288(7) Å, β=91.28(4)°, <I>Z</I>=4, and the final <I>R</I> value obtained was 0.064. The other seven crystals are isomorphous with each other. The central metal atom is in an octahedral hexa-coordination geometry: six nitrogen atoms of isothiocyanate ions are ligated to each metal atom. Each solvent molecule is arranged betweeen each pair of neighboring metal atoms along the [1 \bar1 0] axis in each crystal. The cations are arranged approximately between each pair of metal atoms along the [0 1 1], [0 \bar1 1], and [1 1 0] axes, respectively. They were stable for more than a few weeks at room temperature; however, when heated at about 80–90 °C, their guest molecules were lost.
- 公益社団法人 日本化学会の論文
著者
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Takeuchi Toshio
Department Of Aquatic Biosciences Faculty Of Fisheries Tokyo University Of Fisheries
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Suzuki Yasuo
Department Of Applied Physics Faculty Of Engineering Fukui University
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Ouchi Akira
Department of Chemistry, College of General Education, The University of Tokyo
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Arai Hisanori
Department of Industrial Chemistry, Faculty of Engineering, Meiji University
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Matsumura Naomi
Department of Chemistry, School of Hygienic Sciences, Kitasato University
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Ouchi Akira
Department of Chemistry, College of Arts and Sciences, The University of Tokyo
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