Structure and properties of dichloro(L-proline)cadmium(II) hydrate.
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概要
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An X-ray diffraction study of the title complex has been carried out. The crystal is orthorhombic, with the space group P2<SUB>1</SUB>2<SUB>1</SUB>2<SUB>1</SUB>; <I>Z</I>=4, <I>a</I>=10.021(3), <I>b</I>=13.562(4), <I>c</I>=7.298(3) Å. Block-diagonal least-squares refinements have led to the final <I>R</I> value of 0.035. The structure is very similar to that of dichloro(4-hydroxy-L-proline)cadmium(II), which has a one-dimensional polymer bridged by chlorine atoms and a carboxyl group like an infinite folding screen. The thermal behavior is, however, different from that of dichloro(4-hydroxy-L-proline)cadmium(II). The difference is likely to be due to a difference of the crystal structure, whether it contains intermolecular hydrogen bonds or not.
- 公益社団法人 日本化学会の論文
著者
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Takeuchi Toshio
Department Of Aquatic Biosciences Faculty Of Fisheries Tokyo University Of Fisheries
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Yukawa Yasuhiko
Department of Chemistry, Faculty of Science and Technology, Sophia University
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Inomata Yoshie
Department of Natural Sciences, Faculty of Science and Technology, Sophia University
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Inomata Yoshie
Department of Chemistry, Faculty of Science and Technology, Sophia University
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Takeuchi Toshio
Department of Chemistry, Faculty of Science and Technology, Sophia University
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