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概要
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The crystal and molecular structures of the titled scandium(III) (<B>1</B>) and yttrium(III) chloroacetates (<B>2</B>) were determined by the single-crystal X-ray diffraction method. <B>1</B> is monoclinic, with the space group P2<SUB>1</SUB>/n, <I>a</I>=12.148(4), <I>b</I>=8.860(5), <I>c</I>=11.028(4) Å, and β=103.31(3)°. In <B>1</B>, the metal atom has the hexa-coordinated octahedral geometry, and any pair of the neighboring metal atoms are bridged by three bidentate carboxylate ions, forming an infinite chain. <B>2</B> is isomorphous with the heavy lanthanoid salts, [Ln<SUB>3</SUB>(ClCH<SUB>2</SUB>CO<SUB>2</SUB>)<SUB>9</SUB>(H<SUB>2</SUB>O)<SUB>4</SUB>]<I><SUB>n</SUB></I>·<I>n</I>H<SUB>2</SUB>O (Ln=Gd–Yb), and its crystal structure closely resembles that of the erbium(III) complex.
- 公益社団法人 日本化学会の論文
著者
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Sugita Yoshihiko
Department Of Pathology Aichi-gakuin University School Of Dentistry
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Suzuki Yasuo
Department Of Applied Physics Faculty Of Engineering Fukui University
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Ouchi Akira
Department of Chemistry, College of General Education, The University of Tokyo
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Ohki Yoshiyuki
Department of Industrial Chemistry, Faculty of Engineering, Meiji University
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