Thermospray Liquid Chromatographic/Mass Spectrometric Analysis of Iridoid Glycosides from Gardenia jasminoides

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概要

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• Thermospray liquid chromatography/mass spectrometry (TSP LC/MS) was applied to the determination of iridoid glycosides. Monosaccharide glycosides exhibited dependence, in terms of sensitivity and mass spectra, on the ion source block temperature. Disaccharide glycosides exhibited dependence in sensitivity and peak shape on the block temperature. The resulting mass spectra gave qualitative information concerning both the aglycon and sugar moieties as well as molecular weights. A methanol extract from the fruit of Gardenia jasminoides was analyzed for iridoid glycosides which were identified by mass spectra and mass chromatograms.

• 社団法人日本薬学会の論文
• 1991-08-25

著者

• 井上 謙一郎

  Faculty Of Pharmaceutical Sciences Kyoto University:(present Address)gifu Pharmaceutical University

• 藤多 哲朗

  Faculty of Pharmaceutical Sciences, The University of Tokushima

• 藤多 哲朗

  摂南大学薬学部

• 藤多 哲朗

  Faculty Of Pharmaceutical Sciences Kyoto University

• 藤多 哲朗

  Faculty Of Pharmaceutical Sciences The University Of Tokushima

• 藤多 哲朗

  Kyoto Pharmaceutical Univ. Kyoto Jpn

• 藤多 哲朗

  京大薬

• 飯田 順子

  Analytical Applications Department Shimadzu Corporation

• 小野 正規

  Faculty of Pharmaceutical Sciences, Kyoto University

• 井上 謙一郎

  岐阜薬科大学

• 小野 正規

  Faculty Of Pharmaceutical Sciences Kyoto University

• 藤多 哲朗

  Faculty Of Pharmaceutical Sciences Of Kyoto University

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