Influence of Hydrothermal Conditions on Size of Template Particles for Textured Ceramics
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概要
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We report the influences of the sodium dodecyl-benzenesulfonate (SDBS), hydrothermal reaction temperature and time on the size of potassium sodium niobate (K,Na)NbO3 (KNN) template particles to determine the regularities of these changes. In the reaction with a small autoclave, when the quantity of SDBS reached 1.5 wt %, the width of the obtained platelike KNN-hydrate particles reached a maximum of 1.5 μm and the thickness was 0.15 μm, meaning that the aspect ratio was 10/1. To accommodate practical applications, a large autoclave was used in the following hydrothermal reaction. We found that the size of the platelike particles increased with improved reaction temperature and time. Particles 1.5 to 5 μm wide and 0.15 to 0.4 μm thick were prepared. After calcining these particles at 450 °C, platelike KNN template particles were obtained. Finally, tape-casting results showed that the platelike KNN templates have the (100) orientation.
- 2011-01-25
著者
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Karaki Tomoaki
Department Of Eiectronics And Lnformatics Faculty Of Engineering Toyama Prefectutral Universtiy
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Adachi Masatoshi
Department Of Chemistry And Biotechnology Graduate School Of Engineering Tottori University
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Zhang Fan
School Of Envir & Muni. Eng. Xi'an University Of Architecture & Technology
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Bai Shan
School of Materials Science and Engineering, Shenyang University of Chemical Technology, Shenyang 110142, China
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Bai Shan
School of Materials Science and Engineering, Shenyang Insititute of Chemical Technology, Shenyang 110142, China
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Wen Yuqing
Department of Intelligent Systems Design Engineering, Faculty of Engineering, Toyama Prefectural University, Imizu, Toyama 939-0398, Japan
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Karaki Tomoaki
Department of Intelligent Systems Design Engineering, Faculty of Engineering, Toyama Prefectural University, Imizu, Toyama 939-0398, Japan
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Adachi Masatoshi
Department of Intelligent Systems Design Engineering, Faculty of Engineering, Toyama Prefectural University, Imizu, Toyama 939-0398, Japan
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