Analysis of tin corrosion products using conversion electron Moessbauer spectroscopy, transmission Moessbauer spectroscopy, and X-ray diffractrometry.
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概要
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Tin plates corroded by various acids were nondestructively analyzed by a <SUP>119</SUP>Sn conversion electron Mössbauer spectroscopy, a transmission Mössbauer spectroscopy, and an X-ray diffractometry. The conversion electron method was shown to be useful for analysis of some corrosion products which could not be easily observed by the transmission method. By using both the Mössbauer spectroscopy and the X-ray diffractometry, the corrosion products formed by 6.7M-HNO<SUB>3</SUB>, 5.7M-HCl, and 9.0M-H<SUB>2</SUB>SO<SUB>4</SUB> were determined to be SnO<SUB>2</SUB>·<I>n</I>H<SUB>2</SUB>O, Sn<SUB>4</SUB>(OH)<SUB>6</SUB>Cl<SUB>2</SUB>, and SnSO<SUB>4</SUB>, respectively.
- 公益社団法人 日本化学会の論文
著者
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Endo Kazutoyo
Department Of Physical Chemistry Showa Pharmaceutical University
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Sano Hirotoshi
Deparment of Chemistry, Faculty of Science, Tokyo Metropolitan University
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Shibuya Mamoru
Department of Chemistry, Faculty of Science, Tokyo Metropolitan University
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