Hydrolysis of Acyl Derivatives of Malonaldehyde Dianil. IV. Preparation of β-(p-Toluidino) crotonaldehyde
スポンサーリンク
概要
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β-(p-Toluidino) crotonaldehyde (V), a possible reactant of the Combes reaction, was prepared by the alkaline hydrolysis of β-N-(p-chlorobenzoyl)-p-toluidinocrotonaldehyde (XXIV). Compound XXIV was prepared by the hydrochloric acid-catalyzed hydrolysis of 3-[N-(p-chlorobenzoyl)-p-methylphenylamino]-1-(p-methylphenylimino)-2-butene (XXIII). Compound XXIII was prepared by the alkaline hydrolysis of 1,3-bis [N-(p-chlorobenzoyl)-p-toluidino]-1,3-butadiene (XXII). The alkaline hydrolysis and alcoholysis of 1,3-bis (N-acyl-p-toluidino)-1,3-butadiene (VIII) and the hydrochloric acid-catalyzed hydrolysis of 3-(N-acyl-p-methylphenylamino)-1-(p-methylphenylimino)-2-butene (VI) were examined.
- 社団法人日本薬学会の論文
- 1982-04-25
著者
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尾能 満智子
東邦大薬
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尾能 満智子
School Of Pharmaceutical Sciences Toho University
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田村 眞造
School of Pharmaceutical Sciences, Toho University
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田村 眞造
School Of Pharmaceutical Sciences Toho University
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田村 真造
東邦大学 薬
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