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概要
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The structure of the title complex has been determined by the single-crystal X-ray diffraction method. A crystal of Er<SUB>2</SUB>C<SUB>12</SUB>H<SUB>8</SUB>O<SUB>16</SUB>Cl<SUB>18</SUB>, F. W. 1380.86 is triclinic, with the space group of <I>P</I>\bar1, <I>a</I>=12.787(8), <I>b</I>=15.209(7), <I>c</I>=11.685(7) Å, α=102.24(5), β=114.43(5), γ=70.59(4)°, <I>Z</I>=2 (for the dimer formula), <I>D</I><SUB>x</SUB>=2.36, <I>D</I><SUB>m</SUB>=2.34(3) Mg m<SUP>−3</SUP>, and μ(Mo<I>K</I>α)=5.74 mm<SUP>−1</SUP>. All the carboxylate ions act as bidentate bridges, and each pair of the side-by-side metal atoms is bridged by four carboxylate ions, or by two carboxylate ions and one water-oxygen atom, alternately, forming a polymeric chain approximately parallel to the [011] axis. The chains are arrayed in layers parallel to the (100) plane, and the respective layers are separated by the trichloromethyl groups.
- 公益社団法人 日本化学会の論文
著者
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Imai Takashi
Department Of Bioengineering Faculty Of Bioscience And Biotechnology Tokyo Institute Of Technology
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Ouchi Akira
Department of Chemistry, College of Arts and Sciences, The University of Tokyo
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