Studies of spin labeled sodium dodecyl sulfate. I. Synthesis and properties.
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概要
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Nitroxide spin labeled surfactant, sodium salt of 2-ethyl-2-[9-(hydroxysulfonyloxy)nonyl]-4,4-dimethyloxazolidin-3-yloxyl, was synthesized and some properties of the compound were studied by means of ESR and conductivity measurements. From conductivity measurements it was found that the critical micelle concentration of the compound was 21.6 mmol kg<SUP>−1</SUP> at 25.0±0.1 °C and the micelle consisted of a small number of labeled surfactant ions. The ESR spectra of the labeled surfactant were measured as a function of concentration and temperature. These spectra showed a typical pattern interpreted in terms of spin exchange. Regarding spin exchange as chemical reaction, second order rate constant was determined from the analysis of line width and compared with the values obtained by diffusion controlled model.
- 公益社団法人 日本化学会の論文
著者
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Yamaguchi Takeo
Department Of Chemical System Engineering The University Of Tokyo
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Kimoto Eiji
Department Of Chemistry Faculty Of Science Fukuoka University
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Yamauchi Akira
Department Of Biochemistry Kawasaki Medical Schoo
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Kimizuka Hideo
Department of Chemistry Faculty of Science Kyushu University
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