TG-DTA-MS of Indium Acetate

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概要

• 論文の詳細を見る

• Indium acetate, a promising material for producing indium oxide films (Indium-Tin-Oxide transparent conductive films) by a dip coating, was synthesized and analyzed. The process of oxide formation in nitrogen and helium atmosphere was investigated by so-called TG-DTA-MS, i.e., thermogravimetry (TG) and differential thermal analysis (DTA) coupled with Evolved Gas Analysis (EGA) by mass spectrometry (MS) operated simultaneously. The thermal decomposition proceeded by gas evolution of water vapor and acetic acid followed by gas evolution of acetone and carbon dioxide at the higher temperature. The process in air atmosphere terminated at slightly earlier with an exothermic mass loss accompanying a rapid evolution of acetone, water vapor, and carbon dioxide; the evolved heat by combustion of acetone seemed to accelerate the thermal decomposition. The formula for indium acetate was estimated to be InOH (CH3COO)2 (basic acetate) by which the above reactions were explained satisfactorily.

• 日本質量分析学会の論文
• 1998-08-01

著者

• MATSUSHITA Jun-ichi

  Department of Applied Chemistry, School of Engineering, Tokai University

• OGAWA Makoto

  Department of Nuclear Engineering, School of Engineering, Tokai University

• Matsushita Jun-ichi

  Department Of Applied Chemistry School Of Engineering Tokai University

• SAWADA Yutaka

  Department of Applied Chemistry, Tokyo Institute of Polytechnics

• Seki S

  Department Of Industrial Chemistry Graduate School Of Engineering Tokyo Institute Of Polytechnics

• Sawada Y

  Department Of Industrial Chemistry Graduate School Of Engineering Tokyo Institute Of Polytechnics

• SENDA Tetsuya

  Rigaku Co., Ltd.

• Ogawa M

  Department Of Industrial Chemistry Graduate School Of Engineering Tokyo Institute Of Polytechnic

• SEKI Shigeyuki

  Department of Industrial Chemistry, Graduate School of Engineering, Tokyo Institute of Polytechnics

• SHIGARAKI Taro

  Department of Industrial Chemistry, Faculty of Engineering, Tokyo Institute of Polytechnics

• NISHIDE Toshikazu

  Department of Industrial Chemistry, College of Engineering, Nihon University

• Nishide Toshikazu

  Department Of Industrial Chemistry College Of Engineering Nihon University

• Shigaraki Taro

  Department Of Industrial Chemistry Faculty Of Engineering Tokyo Institute Of Polytechnics

• Senda Tetsuya

  Rigaku Co. Ltd.

• Ogawa Makoto

  Department Of Earth Environment And Resources Sciences Graduate School Of Creative Science And Engin

• Sawada Yutaka

  Department Of Applied Chemistry Faculty Of Engineering Tokyo Institute Of Polytechnics

• Ogawa Makoto

  Department Mechanical Engineering Ii Shibaura Institute Of Technology

• Seki Shigeyuki

  Department of Electronic Engineering, Sendai National College of Technology, 4-16-1 Ayashichuo, Aoba-ku, Sendai 989-3128, Japan

• Nishide Toshikazu

  Department of Chemistry, Faculty of Science, Tohoku University

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