Transmission Electron Microscopy Analysis of Nanorods in BaSnO3-Doped ErBa2Cu3O7-δ Films

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概要

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• Microstructures of BaSnO3-doped ErBa2Cu3O7-δ films were studied by transmission electron microscopy. BaSnO3-doped ErBa2Cu3O7-δ films were grown by a pulsed laser deposition method. In the cross-sectional transmission electron microscopy observation, the presence of nanorods with 10 nm average diameter was confirmed from bright-field images, and these nanorods in turn contained tin (Sn), as confirmed from the energy-dispersive X-ray spectroscopy spectra. The crystal structure of the nanorod was determined to be cubic perovskite from its selected area electron diffraction pattern. Using the selected area electron diffraction patterns, the lattice constant of the nanorods in the ErBa2Cu3O7-δ film was measured to be 0.414 nm. This was in good agreement with the lattice constant of BaSnO3, 0.412 nm. Furthermore, parallel Moiré fringes were observed in the bright-field images, and the relationships between the lattice planes and Moiré fringes were investigated. It was thus confirmed that BaSnO3 was dispersed in the ErBa2Cu3O7-δ as nanorods.

• 2008-02-25

著者

• Kita Ryusuke

  Graduate School Of Electronic Science And Technology Shizuoka University

• ICHINOSE Ataru

  Electrical Physics Department, Komae Research Laboratory, Central Research Institute of Electric Pow

• MUKAIDA Masashi

  Department of Electrical and Information Engineering, Yamagata University

• Matsumoto Kaname

  Department Of Materials Science And Engineering Kyushu Institute Of Technology

• Toh Shoichi

  Hvem Laboratory Kyushu University

• Horii Shigeru

  Department Of Applied Chemistry School Of Engineering University Of Tokyo

• Kato Shingo

  Graduate School Of Materials Science Nara Institute Of Science And Technology

• Teranishi Ryo

  Department Of Materials Science And Engineering Faculty Of Engineering Kyushu University

• Yoshida Yutaka

  Deparlment Of Internal Medicine School Of Medicine Kobe University

• Yamada Kazuhiro

  Department Of Applied Physics And Physico-informatics Faculty Of Science And Technology Keio University

• Matsumoto Kaname

  Department of Materials Science and Engineering, Kyushu Institute of Technology, Kitakyushu 804-8550, Japan

• Yamada Kazuhiro

  Department of Materials Physics and Chemistry, Kyushu University, Fukuoka 819-0395, Japan

• Mukaida Masashi

  Department of Materials Science and Engineering, Kyushu University, Fukuoka 819-0395, Japan

• Kita Ryusuke

  Graduate School of Science and Technology, Shizuoka University, Hamamatsu 432-8561, Japan

• Yasunaga Shuhei

  Department of Materials Physics and Chemistry, Kyushu University, Fukuoka 819-0395, Japan

• Ichinose Ataru

  Electric Power Engineering Research Laboratory, Central Research Institute of Electric Power Industry

• Ichinose Ataru

  Electric Power Engineering Research Laboratory, Central Research Institute of Electric Power Industry, Yokosuka, Kanagawa 240-0196, Japan

• Toh Shoichi

  HVEM Laboratory, Kyushu University, Fukuoka 819-0395, Japan

• Horii Shigeru

  Department of Applied Chemistry, University of Tokyo, Tokyo 113-8656, Japan

• Teranishi Ryo

  Department of Materials Science and Engineering, Kyushu University, Fukuoka 819-0395, Japan

• YAMADA Kazuhiro

  Department of Agricultural Chemistry, Tokyo University of Agriculture

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