HPLC Analysis of Manno-Oligosaccharides Derived from Saccharomyces cerevisiae Mannan Using an Amino Column or a Graphitized Carbon Column

スポンサーリンク

概要

• 論文の詳細を見る

• The chromatographic behavior of manno-oligosaccharides derived from Saccharomyces cerevisiae mannan on two kinds of HPLC columns, an aminopropyl-silica column or a graphitized carbon column(GCC), was investigated. The order of elution of manno-oligosaccharides on both columns with acetonitrile-water was almost the same, that is, the retention increased with increasing molecular size. However, the GCC made it possible to isolate completely two isomers of mannotrioses(M_3-1 and M_3-2)with different linkage positions. We reinvestigated the structures of mannobiose(M_2), M_3s, and mannotetraose(M_4)that were completely isolated by matrix-assisted laser desorption ionization time-of-flight mass spectrometry(MALDI-TOF-MS)and NMR spectroscopy.

• 公益社団法人日本薬学会の論文
• 2002-02-01

著者

• TANIMOTO Toshiko

  School of Pharmaceutical Sciences Mukogawa Women's University

• KOIZUMI Kyoko

  School of Pharmaceutical Sciences, Mukogawa Women's University

• Koizumi K

  School Of Pharmaceutical Sciences Mukogawa Women's University

• Koizumi Kyoko

  School Of Pharmaceutical Sciences Mukogawa Women's University

• IKUTA Akiko

  School of Pharmaceutical Sciences, Mukogawa Women's University

• Sugiyama M

  School Of Pharmaceutical Sciences Mukogawa Women's University

• Ikuta Akiko

  School Of Pharmaceutical Sciences Mukogawa Women's University

• SUGIYAMA Mayumi

  School of Pharmaceutical Sciences, Mukogawa Women's University

• Tanimoto T

  School Of Pharmaceutical Sciences Mukogawa Women's University

• Tanimoto Toshiko

  School Of Pharmaceutical Science Mukogawa Women's University

• Sugiyama Mayumi

  School of Pharmaceutical Sciences, Mukogawa Women's University

関連論文

• Microdose clinical trial : Quantitative determination of fexofenadine in human plasma using liquid chromatography/electrospray ionization tandem mass spectrometry
• Absorption, Distribution and Excretion of β-Cyclodextrin and Glucosyl-β-cyclodextrin in Rats
• Properties and the Inclusion Behavior of 6-O-α-D-Galactosyl- and 6-O-α-D-Mannosyl-cyclodextrins
• Enzymatic Synthesis of N-Acetylglucosaminyl-cyclodextrin by the Reverse Reaction of N-Acetylhexosaminidase from Jack Bean
• Synthesis of 6-O-α-D-Galactosyl α-Cyclodextrin by Coffee Bean α-Galactosidase
• Acceptor Specificity of Cyclodextrin Glycosyltransferase from Bacillus stearothermophilus and Synthesis of α-D-Glucosyl O-β-D-galactosyl-(1→4)-β-D-glucoside
• Galactosylation at Side Chains of Branched Cyclodextrins by Various β-Galactosidases
• Synthesis of Novel Heterobranched β-Cyclodextrins Having β-D-N-Acetylglucosaminyl-Maltotriose on the Side Chain
• Preparation and Characterization of Novel Branched β-Cyclodextrins Having β-D-Galactose Residues on the Non-reducing Terminal of the Side Chains and Their Specific Interactions with Peanut (Arachis hypogaed) Agglutinin
• Synthesis of Novel Heterobranched β-Cyclodextrins from α-D-Mannosyl Maltotriose and β-Cyclodextrin by the Reverse Action of Pullulanase, and Isolation and Characterization of the Products
• Synthesis of Novel Heterobranched β-Cyclodextrins from 4^2-O-β-D-Galactosyl-Maltose and β-Cyclodextrin by the Reverse Action of Pullulanase, and Isolation and Characterization of the Products
• Enzymatic Synthesis of Mannosyl-cyclodextrin by α-Mannosidase from Jack Bean
• Galactosylation of Cyclodextrins and Branched Cyclodextrins by α-Galactosidases
• Acceptor Specificities of α-Mannosidases from Jack Bean and Almond, and Trans-mannosylation of Branched Cyclodextrins
• HPLC Analysis of Manno-Oligosaccharides Derived from Saccharomyces cerevisiae Mannan Using an Amino Column or a Graphitized Carbon Column
• Chemical Structures of Hetero-oligosaccharides Produced by Arthrobacter sp. K-1β- Fructofuranosidase
• Some Properties and the Inclusion Behavior of Three Positional Isomers of 6^1,6^n-Di-O-α-D-glucosyl-cyclomaltoheptaoses (β-Cyclodextrins)
• Avsorption, Distribution and Excretion of Galactosyl-β-cyclodextrin and Mannosyl-β-cyclodextrin in Rats
• Determination of Branched β-Cyclodextrin-Prostaglandin Complexes Using Electrospray Ionization Mass Spectrometry
• Preparation and Characterization of Branched β-Cyclodextrins Having α-_L-Fucopyranose and a Study of Their Functions
• 緒言 : 糖質科学と糖質工学の産業的利用

もっと見る 閉じる

スポンサーリンク