α-Al_2O_3単結晶の高温変形挙動と転位構造(<特集>セラミック材料)

概要

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The structure and glide behavior of basal dislocations in α-Al_O_3 single crystals have been studied by high temperature deformation tests and transmission electron microscopy (TEM). Basal slips were dominant in the deformation at 1400℃ and edge-type basal dislocations belonging to primary slip system were mainly introduced in the sample. On the other hand, rhombohedral twinning formation frequently took place at 1200℃. It was confirmed by high-resolution electron microscopy (HREM) that the basal dislocation dissociates into two half partial dislocations along the [0001] direction. The two partials were separated with a distance of 4.7nm along the [0001] direction and were located at the nearest neighbor positions along the <1l2^^-0> slip direction. This indicates that the basal dislocation dissociates by self-climb perpendicularly to the basal slip plane, and the stacking fault is formed on the {112^^-0} plane between the two partials. However, the two partials are considered to dissociate on the same basal slip plane during deformation because the basal dislocation with climb dissociation can not glide on the basal slip plane.
社団法人日本材料学会の論文
2002-06-15