Microstructures and mechanical properties of TiN-TiB2-Ti5Si3 composites in-situ fabricated by spark plasma sintering

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概要

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• Various TiN-TiB2-Ti5Si3 composites have been synthesized via spark plasma sintering of Ti, BN and Si3N4. The reaction process anlaysis indicates that Ti5Si3 forms earlier than TiB2. The reaction heat as well as the Joule heat may prompt the melting of Ti5Si3, making it infiltrate into TiN and TiB2. Thus, the composites can be further densified with the in-situ addition of Ti5Si3. For TiN-TiB2-Ti5Si3 composites, the maximum fracture toughness was 4.5 ± 0.3 MPa·m1/2, and maximum flexural strength was 601.1 ± 28.5 MPa, which were both quite higher than those of TiN-TiB2 composites. The related toughening and strengthening mechanisms were proposed from microstructural analysis.

• 公益社団法人 日本セラミックス協会の論文

著者

• TU Rong

  Institute for Materials Research, Tohoku University

• GOTO Takashi

  Institute for Materials Research, Tohoku University

• Tu Rong

  Institute For Materials Research Tohoku University

• Jiang Wan

  State Key Lab. Of High Performance Ceramics And Superfine Microstructure Shanghai Inst. Of Ceramics

• Jiang Wan

  State Key Lab Of High Performance Ceramics And Superfine Microstructures Shanghai Institute Of Ceram

• Wang Lianjun

  State Key Lab. For Modification Of Chemical Fibers And Polymer Materials Donghua Univ.

• CHEN Lidong

  State Key Lab of High Performance Ceramics and Superfine Microstructures, Shanghai Institute of Cera

• Chen Lidong

  State Key Lab Of High Performance Ceramics And Superfine Microstructures Shanghai Institute Of Ceram

• ZHANG Jianfeng

  State key Laboratory of High Performance Ceramics and Superfine Microstructure, Shanghai Institute o

• Goto Takashi

  Institute For Material Research Tohoku University

• Liu Leifeng

  State key Laboratory of High Performance Ceramics and Superfine Microstructure, Shanghai Institute o

• Zhang Jianfeng

  Inst. For Materials Res. Tohoku Univ.

• Zhang Jianfeng

  State Key Laboratory Of Elemento-organic Chemistry Research Institute Of Elemento-organic Chemistry

• ZHANG Jianfeng

  State key Laboratory of High Performance Ceramics and Superfine Microstructure, Shanghai Institute of Ceramics, Chinese Academy of Sciences

• LIU Leifeng

  State key Laboratory of High Performance Ceramics and Superfine Microstructure, Shanghai Institute of Ceramics, Chinese Academy of Sciences

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