Studies on Microdetermination of Halogen and Sulfur in Organic Compounds. Tungsten Trioxide, a Novel Catalyst by Combustion Tube Method
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概要
- 論文の詳細を見る
A new method of microdetermination of halogens and sulfur in organic compounds by combustion tube method was examined. It was found that tungsten trioxide among metal oxides was the most appropriate catalyst for oxidation of samples and air as carrier gas was suitable for the analysis. And also, direct introduction of few drops of water into the combustion system was found to be very effective for the analysis. Titration of halogens and sulfur in the combustion product were performed by argentimetric titration at pH 1 with dithizone indicator and by barium perchlorate titration at pH 2 using dinitrosulfonazo-III as indicator, respectively. Whole analysis procedure can be carried out only within 15 minutes.
- 公益社団法人日本薬学会の論文
- 1979-04-25
著者
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小菅 卓夫
静岡薬科大学
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全田 浩
Department Of Pharmacy Shinsyu University Hospital
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小菅 卓夫
Cawthron Institute
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小菅 卓夫
Shizuoka College Of Pharmacy
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全田 浩
Shizuoka College of Pharmacy
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成田 九州男
Shizuoka College of Pharmacy
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成田 九州男
Department of Radiobiochemistry, School of Pharmaceutical Sciences, University of Shizuoka
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全田 浩
信州大学医学部
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成田 九州男
Department Of Radiobiochemistry School Of Pharmaceutical Sciences University Of Shizuoka
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北村 久代
静岡県立大学薬学部
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北村 久代
Shizuoka College of Pharmacy
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北村 久代
静岡県大 薬学部
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