Effects of Silane Coupling Agent Amount on Mechanical Properties and Hydrolytic Durability of Composite Resin After Hot Water Storage
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概要
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The purpose of this study was to evaluate the effects of the silane coupling agent amount on the flexural properties and hydrolytic durability on an experimental composite resin for understanding the optimum amount of silanation. A spherical filler was silanated with 7 different amounts of γ-MPTS, 0, 0.17, 0.34, 0.66, 1.36, 2.72 and 5.45 mass%. Photopolymerized experimental composite resins were made from a 70/30 mass% of UDMA/TEGDMA and a 65 mass% of different silanated amounts of filler. Bar-shaped specimens were prepared for a 3-point bending test in 37℃ water after 1-day water storage at 37℃ and after an additional 1, 7, and 28 days hot water storage in Soxhlet's extractor. The flexural strength and flexural modulus of unsilanated filler dramatically decreased after 28 days hot water storage while those of silanated filler showed a slight change. These results suggested that the silanated amount on the silica filler is not sensitive for flexural properties and hydrolytic stability of composite resin.
著者
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ARKSORNNUKIT Mansuang
Department of Prosthodontics, Faculty of Dentistry, Chulalongkorn University
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TAKAHASHI Hidekazu
Advanced Biomaterials, Graduate School, Tokyo Medical and Dental University
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NISHIYAMA Norihiro
Department of Dental Material, Nihon University School Dentistry at Matsudo
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Arksornnukit Mansuang
Chulalongkorn Univ.
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Takahashi Hidekazu
東京医科歯科大学 医歯学総合研究科包括診療歯科学講座総合診療歯科学
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Nishiyama Norihiro
Department Of Dental Material Nihon University School Of Dentistry At Matsudo
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Nishiyama Norihiro
Department Of Dental Biomaterials Nihon University School Of Dentistry At Matsudo
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Arksornnukit Mansuang
東京医科歯科大学
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Arksornnukit Mansuang
Department Of Prosthodontics Faculty Of Dentistry Chulalongkorn University
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Takahashi H
Department Of Electronics Engineering Faculty Of Engineering Shibaura Institute Of Technology
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Takahashi Hidekazu
Advanced Biomaterials Department Of Restorative Sciences Division Of Oral Health Sciences Graduate S
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Takahashi Hidekazu
Advanced Biomaterials Graduate School Of Medical And Dentistry Tokyo Medical And Dental Univ.
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Takahashi Hidekazu
Advanced Biomaterials Department Of Restorative Sciences Tokyo Medical And Dental University
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Takahashi Hidekazu
Oral Biomaterials Engineering Department Of Oral Materials Sciences And Technology Course Of Oral He
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Takahashi Hidekazu
Advanced Biomaterials Department Of Restorative Science Division Of Oral Health Science Graduate Sch
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Takahashi Hidekazu
Advanced Biomaterials Department Of Restorative Sciences Division Of Oral Health Sciences Graduate S
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