Effects of Heat arid pH in Silanation Process on Flexural Properties and Hydrolytic Durabilities of Composite Resin after Hot Water Storage
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概要
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The objectives of this study were to evaluate the effect of heat application after silanation and the pH effect of silanated solution on flexural properties and hydrolytic durability of experimental composites. A spherical-shaped filler was silanated with 0.66 mass% of γ-MPTS in 70 vol% ethanol solution. For the heating effect, the filler was heated after silanation for 3 hours at 50℃, 80℃ and 110℃. For the effect of pH, ethanol solution with HCl solution of pH 1, 2 and 4 were used. All fillers were mixed to make photopolymerized experimental composite resins. All specimens after immersion in 37℃ water for 24 hours were additionally immersed in Soxhlet's extractor for another 1, 7 and 28 days. A three-point bending test was performed in 37℃ water. The heat application of 50℃ and 80℃ increased flexural strength while heat of 110℃ and pH showed no effects on flexural properties at p<0.05.
- 日本歯科理工学会の論文
著者
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ARKSORNNUKIT Mansuang
Department of Prosthodontics, Faculty of Dentistry, Chulalongkorn University
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TAKAHASHI Hidekazu
Advanced Biomaterials, Graduate School, Tokyo Medical and Dental University
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NISHIYAMA Norihiro
Department of Dental Material, Nihon University School Dentistry at Matsudo
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Arksornnukit Mansuang
Chulalongkorn Univ.
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Takahashi Hidekazu
東京医科歯科大学 医歯学総合研究科包括診療歯科学講座総合診療歯科学
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Nishiyama Norihiro
Department Of Dental Material Nihon University School Of Dentistry At Matsudo
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Nishiyama Norihiro
Department Of Dental Biomaterials Nihon University School Of Dentistry At Matsudo
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Arksornnukit Mansuang
東京医科歯科大学
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Arksornnukit Mansuang
Department Of Prosthodontics Faculty Of Dentistry Chulalongkorn University
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Takahashi H
Department Of Electronics Engineering Faculty Of Engineering Shibaura Institute Of Technology
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PAVASANT v
Department of Anatomy, Faculty of Dentistry, Chulalongkorn University
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Pavasant V
Department Of Anatomy Faculty Of Dentistry Chulalongkorn University
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Takahashi Hidekazu
Advanced Biomaterials Department Of Restorative Sciences Division Of Oral Health Sciences Graduate S
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Takahashi Hidekazu
Advanced Biomaterials Graduate School Of Medical And Dentistry Tokyo Medical And Dental Univ.
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Takahashi Hidekazu
Advanced Biomaterials Department Of Restorative Sciences Tokyo Medical And Dental University
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Takahashi Hidekazu
Oral Biomaterials Engineering Department Of Oral Materials Sciences And Technology Course Of Oral He
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Takahashi Hidekazu
Advanced Biomaterials Department Of Restorative Science Division Of Oral Health Science Graduate Sch
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Takahashi Hidekazu
Advanced Biomaterials Department Of Restorative Sciences Division Of Oral Health Sciences Graduate S
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