Simple and Rapid Determination of Organochlorine Pesticide Residues in Kampo Products by Gas Chromatography/Mass Spectrometry with Negative Chemical Ionization
スポンサーリンク
概要
- 論文の詳細を見る
A simple, rapid and inexpensive sample preparation method using extraction by shaking and sulfuric acid treatment was developed for determining eight organochlorine pesticides in kampo products by gas chromatography/mass spectrometry with negative chemical ionization. The recoveries were between 71% and 117%, and most relative standard deviations were less than 10%. The proposed method was applied to twenty-three samples of kampo formulae, and no samples were contaminated by eight organochlorine pesticides over the quantification limit.
- 公益社団法人 日本薬学会の論文
著者
-
TAGAMI Takaomi
Osaka Prefectural Institute of Public Health
-
KAJIMURA Keiji
Osaka Prefectural Institute of Public Health
-
Sawabe Yoshiyuki
Osaka Prefectural Institute of Public Health
-
Yamasaki Katsuhiro
Osaka Prefectural Institute of Public Health
-
Taguchi Shuzo
Osaka Prefectural Inst. Of Public Health
-
Obana Hirotaka
Osaka Prefectural Inst. Of Public Health
-
Nomura Chie
Osaka Prefectural Institute of Public Health
-
Tagami Takaomi
Osaka Prefectural Inst. Public Health Osaka Jpn
-
Nomura Chie
Osaka Prefectural Inst. Of Public Health
関連論文
- 新規ミニカラム及び光誘導化HPLCによる生落花生, コーン, そば粉及びとうがらし中のアフラトキシンの迅速分析
- Determination of Pyrethroid Pesticides in Cinnamomi Cortex
- Survey of Formaldehyde (FA) Concentration in Cosmetics Containing FA-donor Preservatives
- 室内農薬汚染--ハウスダストに残留するダイアジノン、ペルメトリン及びパラジクロロベンゼン
- Rapid analysis of 56 pesticide residues in natural medicines by GC/MS with negative chemical ionization
- Determination of liothyronine and levothyroxine in dietary supplements by HPLC using a pre-column derivative
- Determination of Liothyronine and Levothyroxine in Dietary Supplements by HPLC Using a Pre-column Derivative
- 大阪府下で1995年から2003年に採取した畜水産食品中の残留合成抗菌剤
- 合成化学物質によるRBL-2H3細胞内のβ-ヘキソサミニダーゼ遊離に対する亜鉛の抑制効果
- 有機塩素系共力剤S-421の魚介類汚染
- ラット好塩基球白血病細胞内のβ-ヘキソサミニダーゼ遊離に及ぼす動物用医薬品の影響
- 新しい残留性有機塩素系環境汚染物質8塩化ジプロピルエーテル(S-421)の水中での分解性
- ラット好塩基球白血病細胞内のβ-ヘキソサミニダーゼ遊離に及ぼす含窒素及びカーバメイト系農薬等の影響
- 二段カートリッジ固相抽出及びオンライン精製HPLCを用いた牛肉及び牛肝臓中のトレンボロン,ゼラノールの迅速分析
- ラット好塩基球白血病細胞内のβ-ヘキソサミニダーゼ遊離に及ぼすピレスロイド系及び有機リン系農薬の影響
- トコフェロールニコチン酸エステルカプセルにおける溶出挙動の経時変化に関する検討
- 無承認無許可医薬品の検査に用いるデータの収集
- LC/MS/MSによる食品中のテトラサイクリン系抗生物質の分析法の検討
- Development of a Method to Reduce Microbial Numbers in Powdered Crude Drugs by a Copper-Alcohol Treatment
- Anti-HIV-1 Activity of Herbs in Labiatae
- Residual Status of Chlorpyrifos and Octachlorodipropylether in Ambient Air and Polished Rice Stock in Houses Five Years after Application for Termite Control
- Inhibitory Effect of Clove Extract on Vero-Toxin Production by Enterohemorrhagic Escherichia coli O157 : H7
- Effects of Preparations of Chinese Medicinal Prescriptions on Digestive Enzymes in Vitro and in Vivo
- Polysaccharide of Astragali Radix Enhances IgM Antibody Production in Aged Mice
- Protective Effect of Astragali Radix by Oral Administration against Japanese Encephalitis Virus Infection in Mice
- Protective Effect of Astragali Radix by Intraperitoneal Injection against Japanese Encephalitis Virus Infection in Mice
- LC/MSを用いた農産物中の17種農薬の残留分析法の検討
- 液-液分配抽出後の含水溶媒に対する無水硫酸ナトリウムの吸水効果
- Determination of Organochlorine Pesticides in Glycyrrhizae Radix
- Determination of Taurine in Energy Drinks by HPLC Using a Pre-column Derivative
- Effects of Temperature during Irradiation on the Production of 2-Alkylcyclobutanones in Beef
- Detection of 2-Alkylcyclobutanones in Irradiated Meat, Poultry and Egg after Cooking
- The Release of Formaldehyde upon Decomposition of 2-Bromo-2-nitropropan-1,3-diol (Bronopol)
- Simple and rapid analysis of aristolochic acid contained in crude drugs and Kampo formulations with solid-phase extraction and HPLC photodiode-array detection
- Simultaneous Analysis of 10 Pyrethroid Pesticides in Natural Medicines by GC/MS with Negative Chemical Ionization
- Rapid Analysis of an Additive Medicinal Ingredient (Dried Thyroid) in Dietary Supplements
- トラネキサム酸カプセルにおける溶出挙動の経時変化に関する検討
- Simple and rapid analysis of sennoside A and sennoside B contained in crude drugs and crude drug products by solid-phase extraction and high-performance liquid chromatography
- Comparative Toxicity in Rats of Polychlorinated Biphenyls (PCBs), Polychlorinated Quaterphenyls (PCQs) and Polychlorinated Dibenzofurans (PCDFs) Present in Rice Oil Causing"Yusho"
- Distribution and Lethal Dose of "Yusho"PCDFs in Cynomolgus Monkeys (Regular Presentations) (Proceedings of the 11 th Symposium on Environmental Pollutants and Toxicology)
- Simultaneous measurement of diazolidinyl urea, urea, and allantoin in cosmetic samples by hydrophilic interaction chromatography
- Photolysis and Antimicrobial Activity of Hinokitiol in Antimicrobial/Deodorant Processed Textiles
- Simple and Rapid Determination of Organochlorine Pesticide Residues in Kampo Products by Gas Chromatography/Mass Spectrometry with Negative Chemical Ionization
- Simple and Rapid Determination of Cypermethrin and Fenvalerate Residues in Kampo Products by Gas Chromatography-Mass Spectrometry with Negative Chemical Ionization
- Screening of Anti-HIV-1 Activity of North American Plants. : Anti-HIV-1 Activities of Plant extracts, and Active Components of Lethalia vulpina (L.) Hue.
- Effects of Astragali Radix from Various Original Plants on Peritoneal Exudate Cell Function in Mice
- Rapid determination of atropine and scopolamine content in scopolia extract powder by HPLC
- Pharmacological Quality of Astragali Radix : The Effect on Antibody Production In Vitro
- Screening of Anti-HIV-1 Activity of North American Plants. Anti-HIV-1 Activities of Plant extracts, and Active Components of Lethalia vulpina (L.) Hue
- Determination of Pyrethroid Pesticides in Cinnamomi Cortex
- Rapid Method for the Determination of 180 Pesticide Residues in Foods by Gas Chromatography/Mass Spectrometry and Flame Photometric Detection