電磁超音波共鳴法によるNi基耐熱合金のクリープ損傷と超音波減衰ピーク

概要

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Electromagnetic acoustic resonance (EMAR) is a contactless resonant method with an electromagnetic acoustic transducer (EMAT). This method is free from extra energy losses, resulting in the measurement of intrinsic ultrasonic attenuation in solids. In this study, the EMAR was applied to detect the creep damage of a Ni-base superalloy (Waspaloy). The material was exposed to the temperature of 1073K at various stresses. We measured ultrasonic attenuation for 1-6-MHz frequency range as the creep advanced. The attenuation coefficient exhibits much larger sensitivity to the damage accumulation than the velocity. In a short interval, between 35% and 40% of whole life, attenuation experiences a large peak and ultrasonic velocity shows a small depression, being independent of the stress. This novel phenomenon is interpreted as resulting from microstructure changes, especially, dislocation mobility. This is supported by TEM observations for dislocation structure. This technique has a potential to assess the damage advance and to predict the creep life of metals.
社団法人日本材料学会の論文
2004-06-15