Acid-Catalyzed Photoreaction of 6-Chloro-1, 3-Dimethyluracil and Mesitylene : Formation of Photocycloadducts and Their Characterization^<1)>

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概要

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• In contrast to the previously reported short time required(1h)for photolysis of 6-chloro-1, 3-dimethyluracil(6-CIDMU)and mesitylene, in the presence of TFA, resulting in two major products : 1, 3, 6, 8, 10-pentamethylcyclooctapyrimidine derivative(1d), and diazapentacyclo[6.4.0.0.^<1, 3>.0^<2, 5>.0^<4, 8>]dodecane(2c), prolonged irradiation(18h)of this same mixture yields novel pentalenopyrimidine derivatives, including diazapentacyclo-[6.4.0.0^<1, 3>.0^<2, 6>.0^<4, 8>]dodecane(3c).

• 公益社団法人日本薬学会の論文
• 2001-04-01

著者

• Seki K

  Central Institute Of Isotope Science (graduate School Of Medicine) Hokkaido University

• OHKURA Kazue

  Faculty of Pharmaceutical Sciences, Health Sciences University of Hokkaido

• Seki Koh-ichi

  Faculty Of Pharmaceutical Sciences Health Sciences University Of Hokkaido

• Ohkura Kazue

  Faculty Of Pharmaceutical Sciences Health Sciences University Of Hokkaido

• Ohkura Kazuto

  Department Of Biological Science And Technology Faculty Of Engineering The University Of Tokushima

• Ohkura Kazuto

  Department Of Applied Biological Sciences School Of Agricultural Sciences Nagoya University

• NISHIJIMA Ken-ichi

  Faculty of Pharmaceutical Sciences, Health Sciences University of Hokkaido

• Ohno Kosei

  Faculty Of Pharmaceutical Sciences Health Sciences University Of Hokkaido

• Okazaki K

  Faculty Of Human Life Science Shikoku University

• Seki Koh-ichi

  Faculty Of Phamaceutical Science Health Sciences University Of Hokkaido

• OHKURA Kazue

  Faculty of Phamaceutical Science, Health Sciences University of Hokkaido

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