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• The crystal structure of TTF·BTDA–TCNQ complex was determined by an X-ray diffraction method. The crystals are monoclinic, space group <I>P</I>2<SUB>1</SUB>⁄<I>n</I> with <I>a</I>=9.660(1), <I>b</I>=7.231(1), <I>c</I>=14.628(2) Å, β=91.31(1)°, and <I>Z</I>=2. The structure was solved by the direct method and refined by the block-diagonal least-squares method to give an <I>R</I> value of 0.040 for non-zero 2620 reflections. The complex is nonionic and the molecules form equally spaced mixed stacks along the b axis. These stacks are connected by strong transverse interactions resulting in a three-dimensional structure. BTDA–TCNQ molecules make cavities by S–N≡C interactions in which TTF molecules are included. This complex is not a simple CT complex with mixed stacks but rather the one with some inclusion behavior.

• 公益社団法人 日本化学会の論文

著者

• Suzuki Takanori

  Deparment Of Biological Science Graduate School Of Science Hiroshima University

• Yamashita Yoshiro

  Department Of Biology Faculty Of Science Kumamoto University

• Kabuto Chizuko

  Instrumental Analysis Center For Chemistry Faculty Of Science Tohoku University

• Mukai Toshio

  Department of Chemistry, Faculty of Science Tohoku University

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