Thienylpyridines as a New Fluorescent Reagent. II. Determination of Carboxylic Acid with 5-(4-Pyridyl)-2-thiophenemethanol Using HPLC.

スポンサーリンク

概要

• 論文の詳細を見る

• The title compound has been prepared and used as a new derivatization reagent. The reagent reacts with the carboxylic acids in chloroform in the presence of 1-isopropyl-3-(3-dimethylaminopropyl)carbodiimide to produce the corresponding fluorescent esters, which can be separated on an octadecyl-silica column. Each 5 fmol of hexadecanoic or octadecanoic acids and about 50 fmol of benzoic and <I>p</I>-anisic acids (1 μl injection) (S/N=2) were detected.

• 公益社団法人 日本化学会の論文

著者

• Nakajima Riichiro

  Department Of Chemical Engineering And Materials Science Faculty Of Engineering Doshisha University

• Fujii Yasuhiro

  Department Of Cardiovascular Surgery Okayama University Graduate School Of Medicine Dentistry And Ph

• Hara Tadashi

  Department Of Chemical Engineering And Materials Sciences Faculty Of Engineering Doshisha University

• Shimada Kazuhiko

  Department Of Obstetrics And Gynecology School Of Medicine Jichi Medical University

• Yamamoto Akifumi

  Department of Applied Chemistry, Faculty of Engineering, Osaka City University

• Shimada Kazuhiko

  Department of Chemical Engineering, Faculty of Engineering, Doshisha University

• Fujii Yasuhiro

  Department of Chemical Engineering, Faculty of Engineering, Doshisha University

関連論文

• Superficial esophageal basaloid squamous cell carcinoma with rare form
• Observation of the complex formation between Cu(II) and protein by capillary electrophoretic system incorporating an UV/CL dual detector
• Selective Detection of Human Serum Albumin Using a Fused-Silica Capillary Modified with Anti-Human Serum Albumin
• α-Amino Acids Analysis by Capillary Electrophoresis with Chemiluminescence Detector Using Luminol-Hydrogen Peroxide-Cu(II) System
• Small-Sized Capillary Electrophoresis with a Chemiliminescence Detector Equipped with Cross-Intersection for Sample Injection
• Analysis of a Biopolymer by Capillary Electrophoresis with a Chemiluminescence Detector Using a Polymer Solution as the Separation Medium
• Influence of Silicon Membrane Interposed between Glass Plates on Microchip Capillary Electrophoresis with a Chemiluminescence Detector
• Migration Behavior of the Polymer Particles Possessing Carboxylate and Borate Moieties in Capillary Electrophoresis
• Improvement of a Capillary Electrophoresis-Chemiluminescence Detection System for Using a Polyacrylamide-Coated Capillary
• Application of Microchip Capillary Electrophoresis with Chemiluminescence Detection to an Analysis for Transition-Metal Ions
• Immunoassay Using Chemiluminescence Detection of Dyestuff-Containing Liposomes as a Labeling Reagent
• Simple and Sensitive Detection Cell for Capillary Electrophoresis-Chemiluminescence Analysis Using Peroxyoxalate Reagent
• Flow-Type Chemiluminescence Detection Cell Using an Optical Fiber for Capillary Electrophoresis
• Design of a Pressure-Mobilization System for Capillary Isoelectric Focusing-Chemiluminescence Detection
• Prevalence of positive FDG-PET findings in patients with high CEA levels
• Analytical Performance of Capillary Electrophoretic System with UV/CL or FL/CL Dual Detector
• Capillary Electrophoresis with Chemiluminescent Detection for Luminol Using Potassium Ferricyanide as a Catalyst
• Clinical significance of performing ^F-FDG PET on patients with gastrointestinal stromal tumors : a summary of a Japanese multicenter study
• High-Sensitivity Determination of Emetine Dithiocarbamate Copper(II) Complex Using the Electrogenerated Chemiluminescence Detection of Tris(2, 2'-bipyridine)ruthenium(II)
• Double-featured Chemiluminescence Reagent Prepared through a Mixing Procedure and Its Application to the Detection of Heme Protein
• Significance of chronic marked hyperglycemia on FDG-PET : is it really problematic for clinical oncologic imaging?
• Diagnostic accuracy of bone metastases detection in cancer patients : Comparison between bone scintigraphy and whole-body FDG-PET
• Effect of chronic hypoxia on left ventricular function in rats
• Photophysics of Structural Color in the Morpho Butterflies
• Reducing the volume of polyethylene glycol electrolyte lavage solution to less than 2 liters for bowel preparation
• Major complications and outcome of diagnostic and operative transvaginal hydrolaparoscopy
• Establishment of criteria for elective single embryo transfer at day 2 or day 3 by analyzing cases with successful implantation of all embryos transferred
• Effects of in vivo exposure to eggs with sperm-immobilizing antibodies in follicular fluid on subsequent fertilization and embryo development in vitro
• Clinical analysis of reflux esophagitis following esophagectomy with gastric tube reconstruction
• Immunohistochemical Mucin Expression of Short-Segment Barrett's Esophagus
• Capillary Electrophoresis-Chemiluminescence Detection System Equipped with a Consecutive Sample-Injection Device
• Correlation Functions of the Asymmetric XXZ Chain and the Painleve V Equation
• Scalar Products of the Asymmetric XXZ Chain
• Spontaneous Magnetization in the Bounded XXZ Spin Chain
• Enhanced Chemiluminescence of Bis(2,4,6-trichlorophenyl) Oxalate - Hydrogen Peroxide - Dyestuff System in the Presence of Polymer Particles
• Micro-channel Chemiluminescence Analysis Using a Peroxyoxalate Reaction that Works through Liquid-Liquid Interface Collapse under Laminar-Flow Conditions
• Effect of Saliva on Measurement of Chemiluminescence by a Micro-Reactor Incorporating a Micro-Channel
• Peak Formation Due to Chemiluminescence Reaction through the Collapse of Laminar Flow Liquid-Liquid Interface in a Microreactor
• Effect of Modified Ultrafiltration on Postoperative Course in Neonates With Complete Transposition of the Great Arteries Undergoing Arterial Switch Operation
• Application of Capillary Electrophoresis with Sensitive Detection to Analysis for Saccharine Molecules
• Tolerance of the developing cyanotic heart to ischemia-reperfusion injury in the rat
• Blunt cardiac rupture in a patient with a history of total correction of tetralogy of Fallot
• Apicoaortic bypass using a vascular graft with a bioprosthetic valve
• Colorectal Perforation Following Retroperitoneal Arterial Reconstruction in a Patient after Pelvic Irradiation
• Successful Treatment of Severe Ischemic Foot Ulcer with Sterile Maggots : The First Case in This Country
• Maggot Debridement Therapy for Severe Diabetic Foot Ulcer
• Direct Observation of Extraction of Cu(II) into Microcapsules Containing 8-Quinolinol by Use of Capillary and Chemiluminescence Detection
• A Case of Superficial Esophageal Cancer Complicated with Idiopathic Muscular Hypertrophy of the Esophagus
• High-Sensitive Analysis of Heme Proteins Separated by Capillary Electrophoresis with On-Line Chemiluminescence Detection Using a Luminol and Hydrogen Peroxide System
• Tuberculosis diagnosed by PCR analysis of synovial fluid
• Simlpe and Convenient Cell for Chemiluminescence Detection in Capillary Electrophoresis
• Electrophoretic Behavior of Dyestuff-Containing Liposome in a Capillary with Original On-Line Chemiluminescence Detection
• Characterization of Dyestuff-containing Liposome by Capillary Zone Electrophoresis Using On-Line Chemiluminescence Detection
• Batch-Type Detection Cell Using a Peroxyoxalate Chemiluminescence System for Capillary Electrophoresis
• Chemiluminescence Detection in Microchip Capillary Electrophoresis
• Separation Behavior of Biological Constituents Having cis-Diol Groups through Interactions with Phenylboronic Acid Sites Introduced on the Inner Wall of a Fused-Silica Capillary
• Chemiluminescence Property of the Luminol-Hydrogen Peroxide-Copper(II)System in the Presence of Surface-Carboxylated Microspheres
• Enhancing Effect of Phenylboronic Acid Compounds and Their Interactions with the Diol Groups of Saccharides in a Capillary Electrophoresis-Chemiluminescence Detection System
• Micro-Flow System Comprised of a Fused-Silica Capillary and Chemiluminescence Detection that Works under Laminar Flow Conditions
• Development of FIA Equipped with a Chemiluminescence Detector Using a Mixed Reagent of Luminol and 1,10-Phenanthroline
• Development of Ultra-micro Flow Analysis with Chemiluminescence Detector
• Capillary Electrophoresis with Chemiluminescence Detector Using On-capillary Detection
• Nonequilibrium Vapor Condensation in Shock Tube
• Preparation of Phenylboronic Acid-Modified Capillary and Separation of Nucleosides by Capillary Electrophoresis
• Performance of a Coiled Capillary of One-cm Diameter in Capillary Electrophoresis
• On-Line Capillary Zone Electrophoretic Separation-Chemiluminescence Detection of Protein Labeled with Fluorescamine
• Electrophoretic Separation and High-Sensitivity Detection of Dyestuff-Labeled Proteins Using an Untreated Fused-Silica Capillary and Sodium Dodecyl Sulfate-Containing Buffer for Migration and Labeling
• Clinical value of FDG-PET for preoperative evaluation of endometrial cancer
• Reaction-Diffusion Processes with Multi-Species of Particles
• Photoacoustic Spectroscopy Theory for Multi-Layered Samples and Interference Effect
• Exact Solution of Riemann-Hilbert Problem for a Correlation Function of the XY Spin Chain : General Physics
• Impact of chronic cyanosis and reoxygenation on the microheterogeneity of the myocardial blood flow : digital radiographic study in neonatal rats
• Pyrolytic sulfurization gas chromatography. XV. Simultaneous determination of the atomic ratio between C,H,O, and N in an organophosphorus compound.
• Pyrolytic sulfurization gas chromatography. XIV. Simultaneous determination of the absolute contents of C, H, O, and N in an organic compound by means of a calibration method.
• Pyrolytic sulfurization gas chromatography. X. The reduction of the analysis time by means of high-frequency heating.
• Pyrolytic sulfurization gas chromatography. XII. The simultaneous determination of the atomic ratio between C,H,O, and N in an organic compound at the centimilligram level.
• Pyrolytic sulfurization gas chromatography. XIII. Simultaneous determination of the atomic ratio between C,H,O, and N in a metal organic chelate compound.
• Pyrolytic sulfurization gas chromatography. XI. An improved apparatus and procedure for practical use.
• Pyrolytic sulfurization gas chromatography. IX. Determination of the atomic ratio between C,H,O,N,Cl,Br,and I in an organic halogen compound.
• Pyrolytic sulfurization gas chromatography. VI. The continuous and simultaneous determination of the atomic ratio between C, H, O, and N in various compounds.
• Pyrolytic sulfurization gas chromatography. VII. The simultaneous determination of the atomic ratio between C, H, O, and N in a halo-organic compound.
• Determination of a small amount of a biological constituent by the use of chemiluminescence. XII. Highly sensitive immunoaffinity chromatography.
• The determination of a small amount of biological constituent by the use of chemiluminescence. VII. An attempt of cyclic immunoaffinity chromatography.
• Thienylpyridines as a new fluorescent reagent. I. Determination of primary alkylamines with 5-(4-pyridyl)-2-thiophenecarbaldehyde using HPLC.
• Pyrolytic sulfurization gas chromatography. II. Simple determination of the correction factors using five standard compounds.
• Pyrolytic sulfurization gas chromatography. III. Simultaneous determination of the atomic ratio between C,H,O, and N in a metallo-organic compound.
• Simultaneous determination of the atomic ratio between C,H,O, and N by the pyrolytic sulfurization method.
• Synthesis and spectral properties of 5,5'-di(4-pyridyl)-2,2'-bithienyl as a new fluorescent compound.
• Immunoassay using a metal-complex compound as a chemiluminescent catalyst. V. Continuous immunoassay by the use of CLCCIA.
• The determination of a small amount of biological constituent by the use of chemiluminescence. V. An iron-dyestuff complex as a catalyst.
• The determination of a small amount of a biological constituent by the use of chemiluminescence. X The determination of protein using a 1,10-phenanthroline-hydrogen peroxide-ruthenium(III) system.
• Improvement in Iron Deficiency Anemia through Therapy with Ferric Ammonium Citrate and Vitamin C and the Effects of Aerobic Exercise.
• On the Ligand Exchange Equilibrium in the Propylene-Mercury(II) Complex
• Thienylpyridines as a New Fluorescent Reagent. II. Determination of Carboxylic Acid with 5-(4-Pyridyl)-2-thiophenemethanol Using HPLC.
• The reductive coupling of organic halide using hydrazine and a palladium catalyst. II. Homocoupling of 1-iodoalkanes.
• Determination of a small amount of a biological constituent by use of chemiluminescence. IX Effect of a ligand on a peak shape.
• Determination of a small amount of a biological constituent by use of chemiluminescence. VIII Effect of heating on the determination of protein.
• Synthesis of Succinonitrile by the Catalytic Reaction of Acrylonitrile in a Gaseous Phase
• A new gas sampler for pyrolytic sulfurization gas chromatography.
• The determination of a small amount of biological constituent by the use of chemiluminescence. IV. A highly sensitive detector for the HPLC of protein.

もっと見る 閉じる

スポンサーリンク