Pyrolytic sulfurization gas chromatography. XIV. Simultaneous determination of the absolute contents of C, H, O, and N in an organic compound by means of a calibration method.
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概要
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The absolute content of C, H, O, and N in an organic compund including a metal organic chelate was satisfactorily determined on the basis of pyrolytic sulfurization gas chromatography. A 1.0–1.3 mg sample was weighed on a microbalance, and was subjected to pyrolytic sulfurization. The gases evolved by the reaction were estimated by gas-chromatography. By using both the analytical result of each product and its calibration factor previously obtained by analyzing cyanoguanidine, 8-quinolinol, and sucrose as standard samples, the absolute content of C, H, O, and N was calculated satisfactorily for each substance.
著者
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Hara Tadashi
Department Of Chemical Engineering And Materials Sciences Faculty Of Engineering Doshisha University
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Okui Fujio
Department of Applied Chemistry, Faculty of Engineering, Doshisha University
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