Optical Resolution of 2-(4-Substituted phenyl)-3-methylbutanoic Acids with Diethylamine by Preferential Crystallization
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概要
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(±-2-(4-Substituted phenyl)-3-methylbutanoic acids (2a-c) were optically resolved by preferential crystallization in the form of their diethylamine salts (3a-c). The molar ratio of the acid to the amine in these salts was found to be 2: 1 by chemical analyses, and was confirmed by analyzing the crystal structure of one of these salts (3b) with X-ray single crystallography.
- 社団法人 日本農芸化学会の論文
著者
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Terunuma Daiyo
Department Of Functional Materials Science Saitama University
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Ito Tasuku
Institute For Molecular Science
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Nohira Hiroyuki
Department Of Applied Chemistry Faculty Of Engineering Saitama University
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Miyashita Akira
Department Of Applied Chemistry Faculty Of Engineering Saitama University
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KOBE Shinzi
Department of Applied Chemistry, Faculty of Engineering, Saitama University
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ASAKURA Ikuko
Department of Applied Chemistry, Faculty of Engineering, Saitama University
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Terunuma Daiyo
Department of Applied Chemistry, Faculty of Engineering, Saitama University
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MIYASHITA Akira
Department of Applied Chemistry, Faculty of Engineering, Saitama University
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