Preparation of Boehmite Sol Employed for Formation of Alumina-Layer over Various Plates with the Dip-Coating
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概要
- 論文の詳細を見る
Formation of boehmite sol from aluminum isopropoxide in aqueous solution was examined with XRD and solid state NMR to reveal that the hydrolysis of the isopropoxide was completed within a rather short reaction time of 1 h while a longer reaction time of 24 h had been employed in the typical preparation procedure. Although it had been mentioned that γ-alumina was formed from the calcination of boehmite at 1073 K, it was suggested that η-alumina, not γ-type, was obtained after the calcination, based on XRD analyses. In order to develop the employment of boehmite sol as the precursor material, the layer of active alumina and its precursor was formed with the dip-coating technique on glass, stainless steel, magnesia and α-alumina plates to show that approximately 1 μm layers were uniformly formed on glass and stainless steel plates while thickness of the layer formed on magnesia and α-alumina was not estimated due to the reflection of uneven plates of those oxides.
- 社団法人 化学工学会の論文
- 2003-09-01
著者
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Hayashi H
Department Of Applied Biological Chemistry Graduate School Of Agricultural And Life Sciences The Uni
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Fujii M
Department Of Chemistry Kyushu School Of Engineering Kinki University
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KAWAKAMI Satoshi
Departments of Urology, Yokohama City University School of Medicine
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Kawakami Satoshi
Department Of Radiology Shinshu University School Of Medicine
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Sugiyama S
Department Of Chemical Science And Technology Faculty Of Engineering The University Of Tokushima
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HAYASHI Hiromu
Department of Chemical Science and Technology, Faculty of Engineering, University of Tokushima
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KUSAKABE Katsuki
Department of Living Environmental Science, Fukuoka Women's University
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FUJII MINAKO
Department of Applied Biochemistry, College of Agriculture, Osaka Prefecture University
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Fujii Minako
Department Of Applied Biochemistry College Of Agriculture Osaka Prefecture University
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Fujii Minako
Department Of Chemical Science And Technology Faculty Of Engineering The University Of Tokushima
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Hayashi Hiromu
Department Of Chemical Science And Technology Faculty Of Engineering The University Of Tokushima
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Sugiyama Shigeru
Department of Advanced Materials, Institute of Technology and Science, The University of Tokushima
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Sugiyama Shigeru
Department Of Advanced Materials Institute Of Technology And Science The University Of Tokushima
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TANIMOTO Shinya
Department of Chemical Science and Technology, Faculty of Engineering, The University of Tokushima
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SHIBAO FUMIO
Department of Applied Chemistry, Graduate School of Engineering, Kyushu University
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Tanimoto Shinya
Department Of Chemical Science And Technology Faculty Of Engineering The University Of Tokushima
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Shibao Fumio
Department Of Applied Chemistry Graduate School Of Engineering Kyushu University
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Kusakabe Katsuki
Department Of Applied Chemistry Graduate School Of Engineering Kyushu University
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Kawakami Satoshi
Department Of Computer Science And Electronics Kyushu Institute Of Technology
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Kusakabe K
Department Of Applied Physics And Chemistry The University Of Electro-communications
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Kawakami Satoshi
Department Of Chemical Science And Technology Faculty Of Engineering The University Of Tokushima
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Shibao F
Department of Applied Chemistry, Graduate School of Engineering, Kyushu University
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林 久治
Department of Chemical Science and Technology, Faculty of Engineering, The University of Tokushima
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