Application of Xanthene Derivatives for Analytical Chemistry, Part LXXXVI. Determination of Rhodium by Third-Derivative Spectrophotometry with o-Hydroxyhydroquinonephthalein in the Presence of N-Hexadecylpyridinium Chloride.
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概要
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A third-derivative spectrophotometric determination (<I>d</I><SUP>3</SUP><I>A</I>⁄<I>d</I>λ<SUP>3</SUP>) of rhodium with <I>o</I>-hydroxyhydroquinonephthalein (Qnph) in the presence of <I>N</I>-hexadecylyridinium chloride (HPC) was proposed by measuring the distance of <I>d</I><SUP>3</SUP><I>A</I>⁄<I>d</I>λ<SUP>3</SUP> on the peak at 530 nm (λ<SUB>3</SUB>) and the troughs at 500 nm (λ<SUB>2</SUB>) and 560 nm (λ<SUB>4</SUB>). Beer's law was valid for the range 0–10 μg rhodium 10<SUP>−1</SUP> cm<SUP>3</SUP>; the apparent molar <I>d</I><SUP>3</SUP><I>A</I>⁄<I>d</I>λ<SUP>3</SUP> was 7.37×10<SUP>5</SUP> dm<SUP>3</SUP> mol<SUP>−1</SUP> cm<SUP>−1</SUP>.
- 公益社団法人 日本化学会の論文
著者
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MORI Itsuo
Osaka College of Pharmacy
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Toyoda Minako
Osaka University of Pharmaceutical Sciences
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Fujita Yoshikazu
Osaka College of Pharmaceutical Sciences
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Maekubo Sachi
Osaka University of Pharmaceutical Sciences
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