SPECTROPHOTOMETRIC DETERMINATION OF ISONIAZID USING FORMATION OF o-HYDROXYHYDROQUINONEPHTHALEIN-PALLADIUM(II)-CETYLTRIMETHYL-AMMONIUM CHLORIDE COMPLEX

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概要

• 論文の詳細を見る

• A simple and highly sensitive spectrophotometric method for the determination of isonicotinic acid hydrazide(isoniazid, INH) using o-hydroxyhydroquinonephthalein(Qn.Ph.)-palladium(II)-cetyl-trimethylammonium chloride(CTAC) complex was established. This method is based on the decrease in the absorbance of Qn.Ph.-palladium (II)-CTAC complex [Qn.Ph. : palladium(II) : CTAC = 3 : 2 : 2] solution. The method could be used in the concentration range of o-1.50 μg/10 ml of INH, where the effective molar "desorptivity" at 635 nm was 6.2 X 10 1 mol^<-1> cm^<-1>. This proposed method was successfully applied to the determination of INH in tablets. The formation of Qn.Ph.-palladium(II)-CTAC complex was studied under various conditions.

• 社団法人日本分析化学会の論文
• 1983-06-05

著者

• FUJITA Yoshikazu

  Osaka University of Pharmaceutical Sciences

• KITANO Shoko

  Osaka College of Pharmacy

• MORI Itsuo

  Osaka College of Pharmacy

• Mori^ Itsuo

  Osaka College Of Pharmacy

• Fujita Yoshikazu

  Osaka College Of Pharmacy

• Fujita Y

  Research And Clinical Laboratory Osaka National Hospital:osaka University Of Pharmaceutical Sciences

• Mori I

  Research And Clinical Laboratory Osaka National Hospital:osaka University Of Pharmaceutical Sciences

• Kitano S

  Osaka College Of Pharmacy

• Fujita Y

  Osaka College Of Pharmacy

• Fujita Yoshikazu

  Osaka College of Pharmaceutical Sciences

関連論文

• Fluorophotometric Determination of Hydrogen Peroxide and Other Reactive Oxygen Species with Fluorescein Hydrazide (FH) and Its Crystal Structure
• SPECTROPHOTOMETRIC DETERMINATION OF VANADIUM WITH GALLEIN AND SODIUM LAURYLSULFATE
• Spectrophotometric Determination of Spermine and Related Compounds Using o-Hydroxyhydroquinonephthalein and Manganese(II)
• SPECTROPHOTOMETRIC DETERMINATION OF BERBERINE CHLORIDE IN PHARMACEUTICAL PREPARATIONS
• SPECTROPHOTOMETRIC DETERMINATION OF GERMANIUM(IV) USING ο-HYDROXYHYDROQUINONEPHTHALEIN AND CETYLPYRIDINIUM CHLORIDE
• COLOR REACTION BETWEEN POLYAMINES AND ο-HYDROXYHYDROQUINONEPHTHALEIN-COPPER(II) COMPLEX
• SPECTROPHOTOMETRIC DETERMINATION OF TUBOCURARINE CHLORIDE USING COLOR REACTION WITH o-HYDROXYHYDROQUINONEPHTHALEIN, ZlRCONIUM(IV) AND FLUORIDE IONS
• Spectrophotometric Determination of Biologically Active Thiols with Eosin, Silver(I)and Adenine
• Spectrophotometric Determination of Ascorbic Acid with Iron(III) and p-Carboxyphenylfluorone in a Cationic Surfactant Micellar Medium
• Spectrophotometric Determination of Gold(III)by an Association Complex Formation between Gold-Thiamine and Phloxine
• Spectrophotometric Determination of Ethylenediaminetetraacetic Acid and Its Related Compounds with p-Carboxyphenylfluorone, Titanium(IV) and Hydrogen Peroxide^1
• Improved o-Sulfophenylfluorone-Titanium(IV) Complex Method for Total Urinary Protein Assay
• Determination of Glycyrrhizinic Acid Based on a Color Reaction with o-Sulfophenylfluorone-Iron(III)Complex
• SPECTROPHOTOMETRIC DETERMINATION OF SULPYRINE USING ο-HYDROXYHYDROQUINONEPHTHALEIN AND CERIUM(IV)
• SPECTROPHOTOMETRIC DETERMINATION OF RESERPINE IN PHARMACEUTICAL PREPARATIONS
• SPECTROPHOTOMETRIC DETERMINATION OF PAPAVERINE WITH o-HYDROXYHYDRO-QUINONEPHTHALEIN AND URANIUM(VI)
• COLOR REACTION BETWEEN PYROGALLOL RED-MOLYBDENUM (VI) COMPLEX AND PROTEIN
• SPECTROPHOTOMETRIC DETERMINATION OF CHLORPHENIRAMINE MALEATE BY COMPLEX FORMATION WITH o-HYDROXYHYDROQUINONEPHTHALEIN, TITANlUM(IV) AND FLUORIDE IN THE PRESENCE OF SODIUM DODECYL SULFATE
• SPECTROPHOTOMETRIC DETERMINATION OF ISONIAZID USING FORMATION OF o-HYDROXYHYDROQUINONEPHTHALEIN-PALLADIUM(II)-CETYLTRIMETHYL-AMMONIUM CHLORIDE COMPLEX
• SPECTROPHOTOMETRIC DETERMINATION OF CHLORPROMAZINE HYDROCHLORIDE USING THE COLOR REACTION WITH PALLADIUM(II) AND o-HYDROXYHYDRO-QUINONEPHTHALEIN
• SPECTROPHOTOMETRIC DETERMINATION OF THIOUREA USING o-HYDROXYHYDROQUINONEPHTHALEIN AND PALLADIUM(II)
• SPECTROPHOTOMETRIC DETERMINATION OF MANGANESE(II) USING o-HYDROXY-HYDROQUINONEPHTHALEIN AND ZEPHIRAMINE
• Spectrophotometric Determination of Uric Acid Based on Fading of o-Hydroxyhydroquinonephthalein-palladium(II)-hexadecyltrimethyl-ammonium Complex
• Spectrophotometric Determination of Glucosamine and Its Analogous Amino Sugars with o-Hydroxyhydroquinonephthalein and Palladium(II)
• Spectrophotometric Determination of Cobalt(II) and Cyanocobalamin with Vanillilfluorone and Its Applications
• Spectrophotometric Determination of DNA Binding Protein, Histone, with 3, 4, 5, 6-Tetrafluoro-2-carboxyphenylfluorone and Manganese(II)^1
• Spectrophotometric Determination of Quinolone Antibiotics by an Association Complex Formation with Aluminum(III) and Erythrosin
• Spectrophotometric Determination of Anthracycline Anticancer Agents with Aluminum(III) and Chromazurol S in a Nonionic Surfactant Micellar Medium
• Determination of Trace Aluminum by Fluorescence Quenching with m-Carboxyphenylfluorone as Analytical Reagent
• Spectrophotometric Determination of Copper(II) with o-Bromophenylfluorone
• Synthesis, Spectral Study and Crystal Structure of a Fluorescein Derivative, p-Methoxycarbonylphenyl Fluorone
• Spectrophotometric Determination of Aluminum with m-Carboxyphenylfluorone, a Novel Chemical Probe, and Its Application
• Spectrophotometric Determination of Micro Amounts of Albumin Using Zirconium(IV) and Xylenol Orange
• Fluorophotometric Determination of Histone with 3,4,5,6-Tetrafluoro-2-carboxyphenylfluorone–Manganese(II) Complex and Its Characterization
• Selective fluorimetric determination of trace amounts of cobalt(II) with the system of fluorescein-hydrogen peroxide-tiron.
• The application of diarylamine compounds in analytical chemistry. 1. Fluorescence reactions among 4-(4-methyl-2-quinolyl)aminosalicylic acid, cobalt(II) and hydrogen peroxide, and the fluorimetry of cobalt(II) by using its fluorescence reaction.
• The sensitive and selective determination of palladium(II) based on ternary-complex formation with phloxine and thiamine.
• Color reaction between indium(III) and o-hydroxyhydroquinonephthalein, and its application.
• The spectrophotometric determination of trace vanadium with 3,4,5,6-tetrachlorogallein.
• Color reaction among pyrogallol red, thorium(IV) and samarium(III), and its application to the determination of these metals.
• Spectrophotometric determination of gentamicin by using a membrane filter preconcentration technique with o-hydroxyhydroquinonephthalein and uranium (VI).
• Determination of titanium(IV) using o-hydroxyhydroquinonephthalein and Tween 20.
• The color reaction of purine bases by ternary-complex formation with eosin and silver(I).
• Application of Xanthene Derivatives for Analytical Chemistry, Part LXXXVI. Determination of Rhodium by Third-Derivative Spectrophotometry with o-Hydroxyhydroquinonephthalein in the Presence of N-Hexadecylpyridinium Chloride.
• The determination of 5-iodouracil using the o-hydroxyhydroquinonephthalein-palladium(II) complex.
• Bio-imaging of hydroxyl radicals in plant cells using the fluorescent molecular probe rhodamine B hydrazide, without any pretreatment(PLANT BIOTECHNOLOGY)

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