Synthesis of Dimeric and Trimeric 2-(<I>p</I>-Tolyloxy)ethyl Acetate-Formaldehyde Polymer Model Compounds

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概要

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• The dimeric and trimeric 2-(<I>p</I>-tolyloxy)ethyl acetateformaldehyde polymer model compounds and the halogenated compound of the dimer were synthesized. 2,2′-Methylenebis(5-methyl-1,2-phenyleneoxy)diethyl acetate was synthesized by the reaction of 2-(<I>p</I>-tolyloxy)ethyl acetate with formaldehyde in acidic media. 2-[2-(2-Acetoxyethoxy-3-chloro-5-methylbenzyl)-4-methylphenoxy]ethyl acetate was prepared by the reaction of 6-chloro-4,4′-dimethyl-2,2′-methylenediphenol with 2-chloroethanol, followed by treatment with acetic anhydride, and 2-[2,6-bis(2-acetoxyethoxy-5-methylbenzyl)-4-methylphenoxy]ethyl acetate from 2,6-bis(2-hydroxy-5-methylbenzyl)-4-methylphenol.

• 公益社団法人 日本化学会の論文

著者

• Matsuda Haruo

  Department Of Applied Chemistry Faculty Of Engineering Osaka University

• Ninagawa Akira

  Department of Applied Chemistry, Faculty of Engineering, Osaka University

• Matsuda Sumio

  Department of Petroleum Chemistry, Faculty of Engineering, Osaka University

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