Systematic Synthesis of Sulfur-containing p-Nitrophenyl α-Maltopentaoside Derivatives for a Differential Assay of Human α-Amylases

スポンサーリンク

概要

• 論文の詳細を見る

• For use in a differential assay of human α-amylases, a variety of 6^5-S-substituted p-nitrophenyl α-maltopentaoside derivatives (6-54) were systematically synthesized via the key intermediate, p-nitrophenyl O-(2,3-di-O-acetyl-6-S-acetyl-4-O-benzoyl-6-thio-α-D-glucopyranosyl)-(1→4)-tris[O-(2,3,6-tri-O-acetyl-α-D-glucopyranosyl)-(1→4)]-2,3,6-tri-O-acetyl-α-D-glucopyranoside (4), which was easily prepared from p-nitrophenyl α-maltopentaoside (G5P) in four steps. The sulfoxide and sulfone derivatives were prepared by oxidizing the corresponding sulfides with m-chloroperbenzoic acid.

• 社団法人日本農芸化学会の論文
• 1993-05-23

著者

• HASEGAWA Akira

  Department of Quantum Science and Energy Engineering, Tohoku University

• KISO Makoto

  Department of Bioorganic Chemistry Gifu University

• Kiso Makoto

  The Foundation For Ume Research Gakuen

• Satomura Shinji

  Osaka Research Laboratories, Wako Pure Chemical Industries

• ISHIDA Hideharu

  Department of Applied Bio-organic Chemistry, Gifu University

• Kiso M

  The Foundation For Ume Research Gakuen

• Satomura Shinji

  Wako Pure Chemical Industries Ltd.

• Satomura Shinji

  Osaka Research Laboratory Wako Pure Chemical Industries Ltd.

• Satomura Shinji

  Osaka Research Laboratories Wako Pure Chemical Industries

• Hasegawa A

  Department Of Applied Bioorganic Chemistry Gifu University

• Kiso Makoto

  ニュージーランド

• Kiso Makoto

  Department Of Applied Bio-organic Chemistry Gifu University

• Ishida H

  Hiroshima Univ. Hiroshima

• Ishida Hideharu

  Faculty Of Appleid Biological Science Gifu University

• Ishida Hideharu

  Department Of Applied Bio-organic Chemistry Gifu University

• Ozawa Kaori

  Department of Applied Bioorganic Chemistry, Gifu University

• Taki Yukako

  Department of Applied Bioorganic Chemistry, Gifu University

• Yamagata Yukari

  Osaka Research Laboratory, Wako Pure Chemical Industries Ltd.

• YAMAGATA Youhei

  Department of Agriscience and Bioscience, Tokyo University of Agriculture and Technology

• Hasegawa Akira

  Department Of Applied Bioorganic Chemistry Gifu University

• Ozawa Kaori

  Department Of Applied Bioorganic Chemistry Gifu University

• Taki Yukako

  Department Of Applied Bioorganic Chemistry Gifu University

• Kitagawa Masayuki

  Department Of Applied Bioorganic Chemistry Gifu University

• Yamagata Yukari

  Laboratory Of Enzymology Graduate School Of Agricultural Science Tohoku University

• Yamagata Y

  Tohoku Univ. Sendai Jpn

• Yamagata Youhei

  Dep. Of Applied Molecular Biology And Biochemistry Tokyo Univ. Of Agriculture And Technol.

• Yamagata Youhei

  Department Of Applied Molecular Biology And Biochemistry Tokyo University Of Agriculture And Technol

• Matsuoka Koji

  Department Of Functional Materials Science Saitama University

• Hasegawa Akira

  Department Of Anesthesiology And Intensive Care Medicine Oita University Faculty Of Medicine

• Hasegawa Akira

  Departmemt Of Information And Imaging Sciences Faculty Of Engineering Chiba University

• Kiso Makoto

  Department Of Applied And Bio-organic Chemistry Gifu University

• Ishida Hideharu

  Department Of Applied And Bio-organic Chemistry Gifu University

• KISO Makoto

  Department of Agricultural Chemistry, Gifu University

• ISHIDA Hideharu

  Department of Agricultural Chemistry, Gifu University

関連論文

• Effect of Specimen Shape on the Low Cycle Fatigue Life of Reduced Activation Ferritic/Martensitic Steel
• lnhibitory action of sulfatide a putative ligand for L-selectiv on B cell proliferation and lg prodrction
• Fatigue Life Assessment Based on Crack Growth Behavior in Reduced Activation Ferritic/Martensitic Steel
• Effect of Changes in Left Ventricular Diastolic Function During Exercise on Exercise Tolerance Assessed by Exercise-Stress Tissue Doppler Echocardiography
• OJ-160 Comparison of Risk Factors between Angiographically Diffuse versus Focal Stenosis in the Patients Enrolled in Japanese Coronary Artery Disease (JCAD) Study(OJ27,Coronary Circulation/Chronic Coronary Disease (Basic/Clinical) (IHD),Oral Presentation
• OE-390 Association between Angiographical Assessment of Luminal Narrowing and Recurrence of Cardiovascular Events : Substudy of Japanese Coronary Artery Disease (JCAD) Study(OE66,Atherosclerosis (Clinical/Pathophysiology) (IHD),Oral Presentation (English)
• Rationale and Design of a Study to Examine Lower Targets for Low-Density Lipoprotein-Cholesterol and Blood Pressure in Coronary Artery Disease Patients : The Japanese Coronary Artery Disease Study II (JCADII)
• High-Temperature Helium Embrittlement of 316FR Steel
• Study on Fatigue Life Evaluation Using Small Specimens for Testing Neutron-Irradiated Materials
• Effects of Doping Elements on Oxidation Properties of Low-Activation Vanadium Alloys
• Improvement of Surface Exfoliation Behavior by Helium-ion Bombardment of a Tungsten Alloy Fabricated by Mechanical Alloying
• Synthetic Studies on Selection Ligands/Inhibitors. Synthesis and Biological Evaluation of Sulfated and Phosphorylated β-D-Galacto- and Lactopyranosides Containing Fatty-Alkyl Residues of Different Carbon Chain Lengths
• SYNTHESIS AND BIOLOGICAL ACTIVITY OF THE NOVEL SULFATED AND PHOSPHORYLATED BIVALENT β-D-GALACTOPYRANOSIDES CONTAINING FATTY-ALKYL RESIDUES
• OJ-383 The effect of ONO-5046 on vascular constrictive remodeling after balloon overstretch injury of rabbit femoral arteries.(Restenosis after Angioplasty, Basic/Clinical 3 (IHD) : OJ46)(Oral Presentation (Japanese))
• A Convenient and Efficient Synthesis of Sialyl Lewis X
• Co- and post-seismic slip associated with the 2005 Miyagi-oki earthquake (M7.2) as inferred from GPS data
• Strain concentration zone along the volcanic front derived by GPS observations in NE Japan arc
• Anesthetic management of laparoscopic adjustable gastric banding in Japanese patients with morbid obesity
• PE-050 Association between Osteopontin-expressing Vascular Smooth Muscle Cells and Non-calcified Unstable Phenotype in Human Atherosclerotic Plaques(Atherosclerosis, clinical-6 (H) PE9,Poster Session (English),The 70th Anniversary Annual Scientific Meetin
• Electrocardiographic Abnormality of Pure Posterior Myocardial Infarction
• PJ-490 Cardiac Sympathetic Nerve Activation Contributes to Manifestation of Connective Tissue Growth Factor and may Promote Myocardial Fibrosis DCM Patients(Heart failure, clinical-13, The 71st Annual Scientific Meeting of the Japanese Circulation Society
• Clinical management and outcome of preemptive renal transplantation in children and adolescents
• Precipitation of Solid Transmutation Elements in Irradiated Tungsten Alloys
• Effects of Transmutation Elements on Neutron Irradiation Hardening of Tungsten
• Fabrication and Characterization of W-Re-Os Alloys for Studying Transmutation Effects of W in Fusion Reactors
• Cavity Formation in a SiC/SiC Composite under Simultaneous Irradiation of Hydrogen, Helium and Silicon Ions
• Improvement of Corrosion Resistance of Vanadium Alloys in High-Temperature Pressurized Water
• Surface Morphology Changes in a SiC/SiC Composite as Caused by Simultaneous Triple-Ion-Beam Irradiation^
• Low Temperature Ductility Loss and Microstructural Evolution of Vanadium-Titanium-Chromium-Silicon Type Alloy after Helium Ion Implantation
• Mechanical Properties of Mo and TZM Alloy Neutron-Irradiated at High Temperatures
• Effect of Helium Implantation on Tensile Properties of V-Ti-Cr-Si Type Alloy
• Self-Consistent Relativistic Linear Augmented Plane Wave Method : Application to YbGa_2
• Relationship between exercise tolerance and TV vs. RR relationship in patients with heart disease
• PJ-584 Effects of Statin Treatment on Cardiac Sympathetic Nerve Activity and Incidence of Cardiac Events in Patients with Acute Myocardial Infarction(Acute myocardial infarction, clinical(diagnosis/treatment)(11)(IHD),Poster Session(Japanese),The 72nd Ann
• PE-421 Geometric adaptation influences exercise tolerance in subjects with preserved systolic function(Exercise test/Cardiac rehabilitation(03)(H),Poster Session(English),The 72nd Annual Scientific Meeting of the Japanese Circulation Society)
• OJ-079 Impact of Insulin Resistance and Chronic kidney Disease on Long-term Patency after Percutaneous Peripheral Intervention(Peripheral circulation/Vascular disease(02)(H),Oral Presentation(Japanese),The 72nd Annual Scientific Meeting of the Japanese Ci
• Autopsy case of systemic sclerosis with severe pulmonary hypertension
• Blood Flow Redistribution During Exercise Contributes to Exercise Tolerance in Patients With Chronic Heart Failure
• PE-170 Rapid and Shallow Breathing Pattern is Influenced by the Compliance of Thorax(Exercise test/Cardiac rehabilitation-4, The 71st Annual Scientific Meeting of the Japanese Circulation Society)
• PJ-183 Rapid and Shallow Breathing Pattern is influenced by Lung Capacity during Exercise(Exercise test/Cardiac rehabilitation-4 (IHD) PJ31,Poster Session (Japanese),The 70th Anniversary Annual Scientific Meeting of the Japanese Circulation Society)
• PJ-038 Diastolic Dysfunction Influences Exercise Tolerance in Subjects with Preserved Systolic Function(Exercise test/Cardiac rehabilitation-5 (IHD) PJ7,Poster Session (Japanese),The 70th Anniversary Annual Scientific Meeting of the Japanese Circulation S
• FRS-033 Expression of Erythropoietin Receptor is Induced in Human Failing Myocardium(Clinical Heart Failure, Diagnosis and Treatment-2 (M) FRS7,Featured Research Session,The 70th Anniversary Annual Scientific Meeting of the Japanese Circulation Society)
• Pleural Effusion at the Onset of Acute Aortic Dissection
• Cholesterol Crystal Embolization : Skin Manifestation, Gastrointestinal and Central Nervous Symptom Treated with Corticosteroid
• Drug eruption due to bosentan in a patient with systemic sclerosis
• Difference between Fresh-Water and Seawater Fishes in the Accumu lation of Environmental Chemical Pollutants
• Studies on the Specificity and Sensitivity of the Influenza C Virus Binding Assay for 9-O-Acetylated Sialic Acids and Its Application to Human Melanomas
• Synthesis of 2-O-Fucosyl Sulfatide, a Blocker of L- and P-Selectin
• Synthesis and Mitogenic Activity of Nonreducing-sugar Subunit Analogs of Bacterial Lipid A Composed only of 3-Hydroxytetradecanoic Acid and Its Homologs
• Synthesis of a Sialyl Lewis X Ganglioside Analogue Containing N-Glycolyl in Place of the N-Acetyl Group in the N-Acetylneuraminic Acid Residue
• Synthesis and Immunoadjuvant Activity of 1-α-O- and 1-β-S-[(3R)-3-Tetradecanoyloxy-tetradecanoyl]-N-acetylmuramoyl-L-alanyl-D-isoglutamine Methyl Esters and Related Compounds
• Systematic Synthesis of Sulfur-containing p-Nitrophenyl α-Maltopentaoside Derivatives for a Differential Assay of Human α-Amylases
• Synthesis and Immunoadjuvant Activity of the Phosphorylated Derivatives of 1-β-S-Acyl- and 6-O-Acyl-1-deoxy-N-acetylmuramoyl-L-alanyl-D-isoglutamine Methyl Esters(Organic Chemistry)
• Synthesis and Immunoadjuvant Activity of 1-α-O-, 1-β-S- and 6-O-(2-Tetra-decylhexadecanoyl) Derivatives of N-Acetylmuramoyl-L-alanyl-D-isoglutamine Methyl Ester(Organic Chemistry)
• Synthesis of Nonreducing-sugar Subunit Analogs of Bacterial Lipid A Carrying the Acyloxyacyl Group of Different Carbon Chain Length(Organic Chemistry)
• Synthesis and Biological Activity of 6-O-(3-Acyloxytetradecanoyl)-N-acetyl-muramoyl Dipeptide Methyl Esters and Related Compounds(Organic Chemistry)
• Synthesis and Immunoadjuvant Activity of N-Acetyl-6-O-phosphono-muramoyl-L-alanyl-D-isoglutamine Methyl Ester and Its Lipophilic Derivatives(Organic Chemistry)
• Synthesis and Immunoadjuvant Activity of the Conjugates of 1-Thio-N-acetyl-muramoyl Dipeptide with Lipid A Subunit Analogs(Organic Chemistry)
• Synthesis of Novel Mycoloyl Derivatives of L-Glucose, 2-Deoxy-D-glucose, D-Glucosamine, and 1,5-Anhydro-D-glucosaminitol(Organic Chemistry)
• Synthesis and Biological Activities of Lipophilic Derivatives of 1-Deoxy-N-acetylmuramoyl-L-alanyl-D-isoglutamine
• Synthesis and Immunoadjuvant Activity of N-[2-O-(1,5-Anhydro-2,3-dideoxy-2-octadecanoylamino-D-glucitol-3-yl)-D-lactoyl]-L-alanyl-D-isoglutamine and Its Derivatives
• Synthesis and Biological Activity of the Lipophilic Derivatives of N-Acetyl-1-thiomuramoyl-L-alanyl-D-isoglutamine(Organic Chemistry)
• First report of a 7-year survey on ABO-incompatible kidney transplantation in Japan
• 乳幼児の腎移植後の頭囲と発達の改善
• Moho and Philippine Sea plate structure beneath central Honshu Island, Japan, from teleseismic receiver functions
• In vitro and in vivo selectin-blocking activities of sulfated lipids nad sulfated sialyl compounds
• Anti-inflammatory effects of sulfatides in selectin-dependent acute lung injury
• Absorption Spectra and Electronic structures in ZnSe-ZnS and ZnTe-ZnSe Strained-layer Superlattices
• Fermi Surface of Th within Local-Density Functional Theory
• Dielectric Behavior and Collective Excitation of an Electron Gas on a Tubule
• Photographic Monitoring under Intravenous Sedation
• Second Harmonic Generation of a Copper Vapor Laser Using an Anamorphic Optical System
• Learning Generalization by Validation Set
• Detection of Cell Membranes in Human Corneal Endothelial Micrograms Using Mathematical Morphology
• Revisiting the three M-7 Miyagi-oki earthquakes in the 1930s : possible seismogenic slip on asperities that were re-ruptured during the 1978 M=7.4 Miyagi-oki earthquake
• Coseismic slip distribution of the 2005 off Miyagi earthquake (M7.2) estimated by inversion of teleseismic and regional seismograms
• Crustal heterogeneity around the Nagamachi-Rifu fault, northeastern Japan, as inferred from travel-time tomography
• High-Temperature Helium Embrittlement of 316FR Steel
• Study on Fatigue Life Evaluation Using Small Specimens for Testing Neutron-Irradiated Materials
• Studies on the Fate of Zn-Diethyldithiocarbamate and Zn-Ethylphenyldithiocarbamate in Rats (Proceedings of the 12 th Symposium on Environmental Pollutants and Toxicology) (Regular Presentations)
• Participation of Hsp72 in DNA Damage by Dimethylarsenics : Possible Relationship between Hsp72 and Apoptosis Induced in Pulmonary Cultured Cells (Proceedings of the 23rd Symposium on Toxicology and Environmental Health)
• Involvement of Metabolic Methylation in Arsenic-Induced Mutagenesis for Mammalian Cells (Proceedings of the 22nd Symposium on Toxicology and Environmental Health)
• Gene Damage in Human Pulmonary Cultured Cells Induced by Dimethylarsenics (Proceedings of the 19th Symposium on Toxicology and Environmental Health)
• Enhancement of the Photocatalytic Reactivity of Unique Rectangular Column-structured TiO_2 Photocatalysts by Incorporating Nanosized Metal Particles
• Hydrodynamic Evolution of Highly Energetic Matter Produced by Cylindrically Symmetric Heavy Ions Collisions
• Quantitative Measurement of Thermal Lens in Diode-Laser Pumped Self-Frequency-Doubled Nd,Lu:YAl_3(BO_3)_4 Laser under Lasing and Non-Lasing Conditions
• Suppression of Self-Frequency-Scanning and Brightness Improvement of a Broad-Stripe Laser Diode using Phase Conjugate Feedback
• Inspiratory Time Effects on Exercise Tolerance in Patients with Chronic Heart Failure(Exercise Training and Cardiac Rehabilitation (H), The 69th Annual Scientific Meeting of the Japanese Circulation Society)
• PJ-490 Abnormal Autonomic Response to Exercise in Diabetic Neuropathy(Exercise Test/Cardiac Rehabilitation 6 (IHD) : PJ82)(Poster Session (Japanese))
• PJ-487 A new Parameter of Rapid & Shallow Breathing Pattern using Cardiopulmonary Exercise test(Exercise Test/Cardiac Rehabilitation 5 (IHD) : PJ81)(Poster Session (Japanese))
• A male patient with malignant lymphoma and thyroid papillary carcinoma after pediatric renal transplantation
• Adult height of three renal transplant patients after growth hormone therapy
• Behavior of Cobalt in Iron- and Steel-making Processes
• The Enhanced Penetration of Oxygen along the Grain Boundary in Semiconducting Barium Titanate
• A Study of Beam-Plasma Discharge. : I. Wave Characteristics
• Synthesis of N-{2-O-[2-Acetamido-1-O-acyl(or 1,6-di-O-acyl)-2,3-dideoxy-α-D-glucopyranose-3-yl]-D-lactoyl}-L-alanyl-D-isoglutamine Methyl Esters, and Their Immunoadjuvant Activities(Organic Chemistry)
• Synthesis of N-[2-O-(2-Acetamido-1,5-anhydro-2,3-dideoxy-D-glucitol-3-yl)-D-lactoyl]-L-alanyl-D-isoglutamine (1-Deoxy-MDP) and Some of Its Lipophilic Analogs, and Their Immunoadjuvant Activities(Organic Chemistry)
• Clinical course of congenital nephrotic syndrome and Denys-Drash syndrome in Japan
• Estimation of damaged tubular epithelium in renal allografts by determination of vimentin expression
• Sotos syndrome associated with complete ureteral duplication and bilateral vesicoureteral reflux

もっと見る 閉じる

スポンサーリンク