Construction of an adiabatic calorimeter workable under constant high-pressure.
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概要
- 論文の詳細を見る
An adiabatic high-pressure calorimeter was constructed. The calorimeter cell was devised for minimization of the cell mass relative to the volume of the sample chamber. The pressure in the cell was controlled by joining the cell with a transmitting tube to a stabilized high-pressure system. The adiabatic conditions were achieved by temperature control of the transmitting tube as well as of adiabatic shields inside the cryostat. Procedures for the precise pressure control and for the determination of the molar volume and heat capacity with the correction for the mass transfer of pressure-transmitting liquid in a series of measurement were discussed. The apparatus is capable of measurement under constant pressure up to 110 MPa and over the temperature range from 100 to 370 K. The results on liquid 3-methylpentane which was used as the pressure medium proved satisfactory performance of this new-type calorimeter.
- 公益社団法人 日本化学会の論文
著者
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Seki Syuzo
Department Of Chemistry Faculity Of Science Osaka University
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Suga Hiroshi
Department Of Chemistry Faculty Of Science Osaka University
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Watanabe Kazuo
Department Of Biology Faculty Of Science Osaka University
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MATSUO Takasuke
Department of Chemistry and Microcalorimetry Research Center, Faculty of Science, Osaka University
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Oguni Masaharu
Department of Chemistry and Chemical Thermodynamics Laboratory, Faculty of Science, Osaka University
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Matsuo Takasuke
Department of Chemistry and Chemical Thermodynamics Laboratory, Faculty of Science, Osaka University
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Suga Hiroshi
Department of Chemistry and Chemical Thermodynamics Laboratory, Faculty of Science, Osaka University
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