Quantitative Determination of Incarvillateine in Incarvillea sinensis by Solid Phase Extraction and High Performance Liquid Chromatography

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概要

• 論文の詳細を見る

• Method for rapid quantitative analysis of incarvillateine in Incarvillea sinensis by high-performance liquid chromatography (HPLC) has been developed. The sample preparation involves solid phase extraction (SPE) with a mixed-mode reversed-phase and cation-exchange cartridge. The linear calibration range for incarvillateine was 0.002-0.5mg/ml. The limit of detection was 0.35μg/ml (S/N=3). Intra- and interday precisions were less than 0.36% (n=6) and 1.61% (n=18), respectively. The recovery of incarvillateine was 97.61-102.44% with the relative standard deviation (RSD) ranging from 0.63 to 1.93% (n=3). This method was proposed as a simple, rapid and accurate method for quantitative determination of incarvillateine content in various samples of Incarvillea sinensis collected from different areas of China.

• 社団法人日本薬学会の論文
• 2005-11-01

著者

• Nohara Toshihiro

  Faculty of Pharmaceutical Sciences, Sojo University

• KINJO Junei

  Faculty of Pharmaceutical Sciences, Fukuoka University

• Nohara T

  Fac. Of Pharmaceutical Sciences Sojo Univ.

• Kinjo Junei

  Faculty Of Pharmaceutical Sciences Fukuoka University

• Kinjo Junei

  Department Of Pharmacognosy Faculty Of Pharmaceutical Sciences Fukuoka University

• Kinjo Junei

  福岡大学 薬学部

• Kinjo Junei

  熊本大学 薬

• Nohara T

  Faculty Of Pharmaceutical Sciences Kumamoto University

• CHI Yu-Ming

  Seiwa Pharmaceutical Ltd.

• NAKAMURA Motoyuki

  Seiwa Pharmaceutical Ltd.

• ZHAO Xi-Ying

  Seiwa Pharmaceutical Ltd.

• YOSHIZAWA Toyokichi

  Seiwa Pharmaceutical Ltd.

• YAN Wen-Mei

  Beijing University of Traditional Chinese Medicine and Pharmacy

• HASHIMOTO Fumio

  Faculty of Pharmaceutical Sciences, Kumamoto University

• CHI Yu

  Seiwa Pharmaceutical, Ltd.

• ZHAO Xi

  Seiwa Pharmaceutical, Ltd.

• YAN Wen

  Beijing University of Traditional Chinese Medicine and Pharmacy

• CHI Yu

  Faculty of Agriculture, Kagoshima University

• Zhao Xi

  Seiwa Pharmaceutical Ltd.

• Yoshizawa Toyokichi

  Seiwa Pharmaceutical Co. Ltd.

• Chi Yu

  Seiwa Pharmaceutical Ltd.

• Hashimoto Fumio

  Faculty Of Pharmaceutical Sciences Kumamoto University

• Hashimoto F

  Faculty Of Agriculture Kagoshima University

• Hashimoto F

  Kagoshima Univ. Kagoshima

• 金城 順英

  熊本大学 薬

• Nakamura M

  Seiwa Pharmaceutical Ltd.

• Jung K

  Laboratory Of Immunomodulator Korea Research Institute Of Bioscience And Biotechnology

• Nohara Toshihiro

  Fac. Of Pharmaceutical Sciences Sojo Univ.

• Kinjo J

  Faculty Of Pharmaceutical Sciences Fukuoka University

• Kim J-h

  Faculty Of Pharmaceutical Sciences Fukuoka University

• Jung K

  Korea Res. Inst. Biosci. And Biotechnol. Taejon Kor

• Hashimoto Fumio

  Department Of Orthodontics Graduate School Of Biomedical Sciences Nagasaki University

• Hashimoto Fumio

  Laboratory Of Ornamental Horticulture Kagoshima University

• Nohara Toshihiro

  Faculty Of Medical And Pharmaceutical Science Kumamoto University

• Nakamura Takanori

  Faculty Of Pharmaceutical Sciences Kumamoto University

• Nakamura Takanori

  Hitachi Zosen Co.

• Nohara T

  Faculty Of Medical And Pharmaceutical Sciences Kumamoto University

• Kinjyo Junei

  Faculty Of Pharmaceutical Sciences Kumamoto University

• Hashimoto Fumio

  Faculity Of Science Osaka City University

• Nakamura Takanori

  Faculty of Medical and Pharmaceutical Sciences, Kumamoto University

• Nohara Toshihiro

  Faculty of Medical and Pharmaceutical Scieces, Sojo University

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