Studies on the Synthesis of 4-Methoxypyrimidine 1-Oxide and its Reissert Reaction.
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4-Methoxypyrimidine 1-oxide was prepared and its Reissert reaction afforded 4-methoxypyrimidine-2-carbonitrile, which was derived to 2,4-dimethoxypyrimidine to confirm the structure. At the same time, difference in the nucleophilic activity of the 2-and 4-positions in pyrimidine 1-oxide was clarified. During the course of this work, a simple process for the preparation of 4-methoxypyrimidine was established.
- 公益社団法人日本薬学会の論文
- 1959-05-10
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