Preparation of graphite fluoride by vertical vibrating reactor.
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概要
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A study was made of the yield and crystallinity of graphite fluoride using a vertical vibrating reactor, which made it possible to prepare much graphite fluoride. The yield of graphite fluoride decreased beyond 500 °C for natural graphite and petroleum coke heat-treated at 2800 °C, and beyond 300 °C for calcined petroleum coke. The crystallinity of graphite fluoride was improved through the decomposition and refluorination process in these temperature ranges where the yield decreased. It was found that a sublimative solid by-product was formed together with gaseous fluorocarbons. It was a white solid fluorocarbon with 5–9 cyclohexane rings.
- 公益社団法人 日本化学会の論文
著者
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Watanabe Nobuatsu
Department of Industrial Chemistry, Faculty of Engineering, Kyoto University
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Nakajima Tsuyoshi
Department of Applied Chemistry, Graduate School of Engineering, Tokyo University of Agriculture and Technology, Koganei, Tokyo 184-8588, Japan
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Katoh Saburo
Department of Industrial Chemistry, Faculty of Engineering, Kyoto University
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