Combination treatment of tribochemical treatment and phosphoric acid ester monomer of zirconia ceramics enhances the bonding durability of resin-based luting cements
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概要
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The aim of the present study was to evaluate the bonding durability of resin-based luting cement to partially stabilized tetragonal zirconia (Y-TZP) achieved by combination treatment of tribochemical (TBC) treatment and two different phosphate acid ester monomers. Two phosphate acid ester monomers (EP: Epricord opaque primer, AZ: AZ primer) were applied to each surface modification followed by application of resin-based luting cement (Rely-X ARC). Bonding specimens were placed in deionized water at 37°C and stored for 24 h. The other groups were subjected to 30,000 cycles of a thermal stress for the durability test. Shear bond tests were done using a universal testing machine at 1 mm/min. Shear bond strengths of combination treatments using EP and AZ on TBC treatment after thermal stress showed no significant difference (p>0.05) compared with those of storage after 24 h. Combination treatment using phosphoric acid ester monomer could achieve a durable bond.
著者
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TAKEUCHI Kenichiro
Department of Oral Biomaterials and Technology, School of Dentistry, Showa University
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FUJISHIMA Akihiro
Department of Oral Biomaterials and Technology, School of Dentistry, Showa University
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MANABE Atsufumi
Division of Aesthetic Dentistry, Showa University School of Dentistry
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KURIYAMA Soichi
Department of Oral Biomaterials and Technology, School of Dentistry, Showa University
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HOTTA Yasuhiro
Department of Oral Biomaterials and Technology, School of Dentistry, Showa University
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TAMAKI Yukimichi
Department of Oral Biomaterials and Technology, School of Dentistry, Showa University
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MIYAZAKI Takashi
Department of Oral Biomaterials and Technology, School of Dentistry, Showa University
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