Metal Compound Analysis by Capillary Chromatography Using an Untreated Capillary Tube and Water-Hydrophilic-Hydrophobic Solvent Mixture as a Carrier Solution
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概要
- 論文の詳細を見る
A tube radial distribution chromatography (TRDC) system was developed using an untreated open capillary tube and a water-hydrophilic-hydrophobic solvent mixture as a carrier solution. We examined metal compounds such as copper(II) sulfate, hematin, and hemoglobin using the TRDC system equipped with a chemiluminescence detector. The model mixture solutions of hematin–copper(II), and hemoglobin–copper(II), were injected into a fused-silica capillary tube by the gravity method and subsequently delivered with the carrier solutions of water–acetonitrile–ethyl acetate (2:7:4 volume ratio) and water–acetonitrile–ethyl acetate (15:2:1 volume ratio), respectively, using a microsyringe pump. The mixture of hematin–copper(II) as well as hemoglobin–copper(II) was well separated and eluted with the organic solvent-rich carrier solution based on the tube radial distribution and detected by chemiluminescence in the present TRDC system.
著者
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Tsukagoshi Kazuhiko
Department of Chemical Engineering and Materials Science, Faculty of Engineering, Doshisha Universit
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塚越 一彦
Department Of Chemical Engineering And Materials Science Doshisha University
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Tsukagoshi Kazuhiko
Department Of Chemical Engineering And Materials Science Faculty Of Engineering Doshisha University
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Tsukagoshi Kazuhiko
Department Of Chemical Engineering And Materials Science Faculty Of Science And Engineering Doshisha
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Tsukagoshi K
Doshisha Univ. Kyoto Jpn
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Tsukagoshi Kazuhiko
Dep. Of Chemical Engineering And Materials Sci. Fac. Of Engineering Doshisha Univ. Kyotanabe Kyoto 6
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Tsukagoshi K
Doshisha Univ. Kyotanabe
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塚越 一彦
Department Of Chemical Engineering And Materials Science Faculty Of Engineering Doshisha University
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Hashimoto M
Department Of Polymer Science And Engineering Faculty Of Textile Science Kyoto Institute Of Technolo
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Tsukagoshi Kazuhiko
Department Of Chemical Engineering And Materials Science Faculty Of Science And Engineering Doshisha
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Jinno Naoya
Department Of Chemical Engineering And Materials Science Faculty Of Science And Engineering Doshisha
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Hashimoto Masahiko
Department Of Chemical Engineering And Materials Science Faculty Of Science And Engineering Doshisha
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Yoshida Kazuma
Department Of Chemical Engineering And Materials Science Faculty Of Science And Engineering Doshisha University
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Tsukagoshi Kazuhiko
Doshisha Univ. Kyoto Jpn
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Tsukagoshi Kazuhiko
Department Of Chemical Engineering And Materials Science Doshisha University
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