Immobilized Triazine-Type Dehydrocondensing Reagents for Carboxamide Formation: ROMP-Trz-Cl and ROMP(OH)-Trz-Cl

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概要

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• New triazine-type dehydrocondensing reagents, such as ROMP-Trz-Cl and ROMP(OH)-Trz-Cl, were synthesized by a ring opening metathesis polymerization (ROMP) method, and these showed higher loading than conventional polymer-supported condensing reagents. These polymers effect the formation of amides in good yields by addition of a mixture of carboxylic acid, amine and NMM. ROMP(OH)-Trz-Cl, which contains hydroxyl groups in the polymer chain, gave amides in good yields even in MeOH.

• 公益社団法人日本薬学会の論文
• 2007-05-01

著者

• TANI Shohei

  Faculty of Pharmaceutical Sciences and High Technology Research Center, Kobe Gakuin University

• Tani S

  Faculty Of Pharmaceutical Sciences Kobe Gakuin University

• Hioki K

  Faculty Of Pharmaceutical Sciences Kobe Gakuin University22:09:10life Science Center Kobe Gakuin Uni

• Hioki Kazuhito

  Faculty Of Pharmaceutical Sciences Kobe Gakuin University

• Kunishima M

  Faculty Of Pharmaceutical Sciences Kobe Gakuin University:life Science Center Kobe Gakuin University

• Kunishima Munetaka

  Faculty Of Pharmaceutical Sciences Institute Of Medical Pharmaceutical And Health Sciences Kanazawa

• Kunishima Munetaka

  Faculty Of Pharmaceutical Sciences Kobe Gakuin University

• KAMEYAMA Satomi

  Faculty of Pharmaceutical Sciences, Kobe Gakuin University

• Kameyama Satomi

  Faculty Of Pharmaceutical Sciences Kobe Gakuin University

関連論文

• Direct Preparation of Primary Amides by Reaction of Carboxylic Acids and Ammonia in Alcohols Using DMT-MM
• Reduction of Acetals with Samarium Diiodide in Acetonitrile in the Presence of Lewis Acids
• Coupling Reaction of Vinyl Halides with Ketones or Aldehydes Mediated by Samarium Diiodide
• [2, 3]-Wittig Rearrangement Initiated by 1, 5-Hydrogen Atom Transfer from an o-Iodophenyl Group on the α-Carbon of Allylic Ethers by Reduction with SmI_2
• REDUCTION OF DITHIOACETALS WITH SmI_2 IN BENZENE-HMPA
• A Racemization Test in Peptide Synthesis Using 4-(4,6-Dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium Chloride (DMT-MM)
• Benzyl 4,6-Dimethoxy-1,3,5-triazinyl Carbonate as N-Protecting Reagent
• Development of Novel Polymer-type Dehydro- condensing Reagents Comprised of Chlorotriazines
• Halogenolactamization of 2-(3-Butenyl)-1,3-oxazolines to Bifunctional γ-and δ-Lactams
• Immobilized Triazine-Type Dehydrocondensing Reagents for Carboxamide Formation: ROMP-Trz-Cl and ROMP(OH)-Trz-Cl
• Development of a Simple System for Dehydrocondensation Using Solid-Phase Adsorption of a Water-Soluble Dehydrocondensing Reagent (DMT-MM)
• Preparation of Weinreb Amides Using 4- (4, 6-Dimethoxy-1, 3, 5-triazin-2-yl) -4-methylmorpholinium Chloride (DMT-MM)
• Convenient One-Pot Synthesis of 2-Oxazolines from Carboxylic Acids
• One-Pot Preparation of Oxazol-5(4H)-ones from Amino Acids in Aqueous Solvents

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