Synthesis of 2,4-di(p-formyl)-.ALPHA.-truxillic acid by crystal engineering.
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概要
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<I>p</I>-Formycinnamic acid, which usually crystallizes in either the β-form or γ-form of packing, was converted into its diethyl acetal. The introduction of such bulky groups onto a benzene ring successfully provided us with the α-form of packing, from which the desired photodimer, 2,4-di(<I>p</I>-formyl)-α-truxillic acid (<I>c</I>-2, <I>t</I>-4-bis(<I>p</I>-formylphenyl)-<I>r</I>-1,<I>t</I>-3-cyclobutanedicarboxylic acid) was obtained with a yield of 85–90%.
- 公益社団法人 日本化学会の論文
著者
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NAKANISHI Hachiro
Research Institute for Polymers and Textiles
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Nakanishi Fusae
Research Institute for Polymers and Textiles
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Ishii Michiko
Research Institute for Polymers and Textiles
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