Gas chromatography-mass spectrometry of N-trifluoroacetyl trimethylsilyl esters of some iminodicarboxylic acids.
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概要
- 論文の詳細を見る
The simultaneous <I>N</I>-trifluoroacetylation and <I>O</I>-trimethylsilylation of some iminodicarboxylic acids were studied by the use of a mixture of α,α,α,α′,α′,α′-hexafluoro-<I>N</I>-methyldiacetamide and <I>N</I>,<I>O</I>-bis(trimethylsilyl)trifluoroacetamide, as a derivatizing reagent. The resulting <I>N</I>-trifluoroacetyl trimethylsilyl ester derivatives gave rather complicated mass spectra with molecular (M<SUP>+</SUP>) and M–15 (loss of CH<SUB>3</SUB>) ions upon electron impact at 20 eV.
- 公益社団法人 日本化学会の論文
著者
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Morimoto Shiro
Department Of Pharmacology Osaka College Of Pharmacy
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Yoshida Hideyuki
Department of Chemical Engineering, Faculty of Engineering, Tokushima University
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Kawashiro Katsuhiro
Department of Chemical Engineering, Faculty of Engineering, Tokushima University
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