Reaction of dimethyl phosphonate with ketene dimethyl dithioacetal derivatives. An alternative method to prepare s-alkylphosphonates.
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概要
- 論文の詳細を見る
Reaction of dimethyl phosphonate with phenylketene dimethyl dithioacetal derivatives have been investigated to prepare <I>s</I>-alkylphosphonates. The addition reactions of phosphonate were accelerated in dithioacetal derivatives in the following order: –SMe<–SOMe<<–SO<SUB>2</SUB>Me. The reaction of β,β-bis(methylsulfonyl)styrene (<B>7</B>) with dimethyl phosphonate followed by the catalytic reduction afforded dimethyl α-methylbenzylphosphonate in 74% yield from compound <B>7</B>. The reaction of 1-methylsulfinyl-1-methylthio-4-phenyl-1-butene with dimethyl phosphonate gave dimethyl (2-methylthio-1-phenethylvinyl) phosphonate in 21% yield.
- 公益社団法人 日本化学会の論文
著者
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Watabe Takashi
Department Of Radiology Saitama Medical School
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Yoshida Hiroshi
Departmen Of Radiology School Of Medicine Asahikawa Medical University
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Inokawa Saburo
Department of Chemistry Faculty of Science Kyoto University
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Inokawa Hiromi
Department of Chemistry Faculty of Science Kyoto University
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Ogata Tsuyoshi
Department of Applied Chemistry, Faculty of Engineering, Shizuoka University
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Watabe Takashi
Department of Synthetic Chemistry, Faculty of Engineering, Shizuoka University
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Yamashita Mitsuji
Deparment of Applied Chemistry, Faculty of Engineering, Shizuoka University
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Miyano Tadaaki
Department of Synthetic Chemistry, Faculty of Engineering, Shizuoka University
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Inokawa Hiromi
Department of General Education, Shizuoka Women's Junior College
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- Reaction of dimethyl phosphonate with ketene dimethyl dithioacetal derivatives. An alternative method to prepare s-alkylphosphonates.